2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranosyl (N-phenyl)trifluoroacetimidate

Base Information

Chemical Name:2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranosyl (N-phenyl)trifluoroacetimidate
CAS No.:590367-96-7
Molecular Formula:C₆₉H₅₄F₃NO₁₈
Molecular Weight:1242.18
Hs Code.:

Synonyms:2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranosyl (N-phenyl)trifluoroacetimidate

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Chemical Property of 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranosyl (N-phenyl)trifluoroacetimidate

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Technology Process of 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranosyl (N-phenyl)trifluoroacetimidate

There total 4 articles about 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranosyl (N-phenyl)trifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 61881-19-4
2,2,2-trifluoro-N-phenyl-acetimidoyl chloride

: 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranoside

: 590367-96-7
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranosyl (N-phenyl)trifluoroacetimidate

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃;
DOI:10.1021/jo034223u

Reference yield:

: 590367-95-6
1,2,3,4-tetra-O-benzoyl-D-glucopyranoside

: 590367-96-7
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranosyl (N-phenyl)trifluoroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / TMSOTf; molecular sieves 4 Angstroem / CH₂Cl₂ / 8 h / 20 °C

2: 67 percent / NH₃ / methanol; tetrahydrofuran / 22 h / 0 - 20 °C

3: 99 percent / K₂CO₃ / acetone / 20 °C

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; ammonia; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1021/jo034223u

Reference yield:

: 339276-12-9
2,3,4,6-tetra-O-benzoyl-D-glucopyranosyl 1-(N-phenyl)-2,2,2-trifluoroacetimidate

: 590367-96-7
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzoyl-D-glucopyranosyl (N-phenyl)trifluoroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / TMSOTf; molecular sieves 4 Angstroem / CH₂Cl₂ / 8 h / 20 °C

2: 67 percent / NH₃ / methanol; tetrahydrofuran / 22 h / 0 - 20 °C

3: 99 percent / K₂CO₃ / acetone / 20 °C

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; ammonia; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1021/jo034223u