C₃₇H₄₄N₂O₉S

Base Information

Chemical Name:C₃₇H₄₄N₂O₉S
CAS No.:1374768-69-0
Molecular Formula:C₃₇H₄₄N₂O₉S
Molecular Weight:692.83
Hs Code.:

C<sub>37</sub>H<sub>44</sub>N<sub>2</sub>O<sub>9</sub>S

Synonyms:C₃₇H₄₄N₂O₉S

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Chemical Property of C₃₇H₄₄N₂O₉S

Chemical Property:

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Technology Process of C₃₇H₄₄N₂O₉S

There total 13 articles about C₃₇H₄₄N₂O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374768-68-9
tert-butyl 2-(benzyloxy)ethyl((3aR,5R,6S,7R,7aR)-5-(hydroxymethyl)-6,7-bis(4-methoxybenzyloxy)-5,6,7,7a-tetrahydro-3aH-pyrano[3,2-d]thiazol-2-yl)carbamate

: 1374768-69-0
C₃₇H₄₄N₂O₉S

Guidance literature:: With N-Bromosuccinimide; potassium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; In dichloromethane; water; at 0 - 20 ℃; for 0.5h;

Reference yield:

: 14131-63-6
D-glucosamine hydrochloride

: 1374768-69-0
C₃₇H₄₄N₂O₉S

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydroxide / 20 °C

2.1: pyridine

3.1: hydrogenchloride; water / acetone

4.1: sodium hydrogencarbonate / dichloromethane; water

5.1: dichloromethane / 2 h / 0 °C

5.2: 12 h / 20 °C

5.3: Cooling with ice

6.1: potassium carbonate; methanol / 3 h / 20 °C

7.1: triethylamine / methanol / 5 h / 20 °C

8.1: triethylamine / dmap / dichloromethane / 12 h / 20 °C

9.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

9.2: 1.5 h / 15 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

11.1: N-Bromosuccinimide; potassium hydrogencarbonate / tetrabutylammomium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 0.5 h / 0 - 20 °C

With pyridine; hydrogenchloride; methanol; N-Bromosuccinimide; tetrabutyl ammonium fluoride; water; sodium hydride; sodium hydrogencarbonate; potassium carbonate; potassium hydrogencarbonate; triethylamine; sodium hydroxide; dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; mineral oil;

Reference yield:

: 7597-81-1
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(4-methoxybenzylidene)amino-β-D-glucopyranose

: 1374768-69-0
C₃₇H₄₄N₂O₉S

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogenchloride; water / acetone

2.1: sodium hydrogencarbonate / dichloromethane; water

3.1: dichloromethane / 2 h / 0 °C

3.2: 12 h / 20 °C

3.3: Cooling with ice

4.1: potassium carbonate; methanol / 3 h / 20 °C

5.1: triethylamine / methanol / 5 h / 20 °C

6.1: triethylamine / dmap / dichloromethane / 12 h / 20 °C

7.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

7.2: 1.5 h / 15 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

9.1: N-Bromosuccinimide; potassium hydrogencarbonate / tetrabutylammomium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 0.5 h / 0 - 20 °C

With hydrogenchloride; methanol; N-Bromosuccinimide; tetrabutyl ammonium fluoride; water; sodium hydride; sodium hydrogencarbonate; potassium carbonate; potassium hydrogencarbonate; triethylamine; dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; mineral oil;