(E)-4,4,4-trifluoro-3-(dimethylphenylsilyl)-1-(4-methoxyphenyl)-2-buten-1-yl methoxymethyl ether

Base Information

Chemical Name:(E)-4,4,4-trifluoro-3-(dimethylphenylsilyl)-1-(4-methoxyphenyl)-2-buten-1-yl methoxymethyl ether
CAS No.:1147879-69-3
Molecular Formula:C₂₁H₂₅F₃O₃Si
Molecular Weight:410.508
Hs Code.:

Synonyms:(E)-4,4,4-trifluoro-3-(dimethylphenylsilyl)-1-(4-methoxyphenyl)-2-buten-1-yl methoxymethyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4,4,4-trifluoro-3-(dimethylphenylsilyl)-1-(4-methoxyphenyl)-2-buten-1-yl methoxymethyl ether

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Technology Process of (E)-4,4,4-trifluoro-3-(dimethylphenylsilyl)-1-(4-methoxyphenyl)-2-buten-1-yl methoxymethyl ether

There total 1 articles about (E)-4,4,4-trifluoro-3-(dimethylphenylsilyl)-1-(4-methoxyphenyl)-2-buten-1-yl methoxymethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1147880-08-7
(E)-4,4,4-trifluoro-1-(4-methoxyphenyl)-3-dimethylphenylsilyl-2-buten-1-ol

: 107-30-2
chloromethyl methyl ether

: 1147879-69-3
(E)-4,4,4-trifluoro-3-(dimethylphenylsilyl)-1-(4-methoxyphenyl)-2-buten-1-yl methoxymethyl ether

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/b819476a

Reference yield: 72.0%

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 1147879-69-3
(E)-4,4,4-trifluoro-3-(dimethylphenylsilyl)-1-(4-methoxyphenyl)-2-buten-1-yl methoxymethyl ether

: 2-(trifluoromethyl)-1-{4-(trifluoromethyl)phenyl}-4-(methoxymethyl)oxy-4-(4-methoxyphenyl)-2-buten-1-ol

Guidance literature:: With tetrabutyl ammonium fluoride; zinc trifluoromethanesulfonate; In 1-methyl-pyrrolidin-2-one; at 80 ℃; for 20h; Inert atmosphere;
DOI:10.1039/b819476a

Reference yield: 59.0%

: 1147879-69-3
(E)-4,4,4-trifluoro-3-(dimethylphenylsilyl)-1-(4-methoxyphenyl)-2-buten-1-yl methoxymethyl ether

: 104-88-1
4-chlorobenzaldehyde

: 1-(4-chlorophenyl)-2-(trifluoromethyl)-4-(methoxymethyl)oxy-4-(4-methoxyphenyl)-2-buten-1-ol

Guidance literature:: With tetrabutyl ammonium fluoride; zinc trifluoromethanesulfonate; In 1-methyl-pyrrolidin-2-one; at 80 ℃; for 20h; Inert atmosphere;
DOI:10.1039/b819476a