C₄₃H₆₀O₁₂

Base Information

Chemical Name:C₄₃H₆₀O₁₂
CAS No.:476687-99-7
Molecular Formula:C₄₃H₆₀O₁₂
Molecular Weight:768.942
Hs Code.:

C<sub>43</sub>H<sub>60</sub>O<sub>12</sub>

Synonyms:C₄₃H₆₀O₁₂

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Chemical Property of C₄₃H₆₀O₁₂

Chemical Property:

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Technology Process of C₄₃H₆₀O₁₂

There total 37 articles about C₄₃H₆₀O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 476687-97-5
C₆₅H₁₁₂O₁₂Si₄

: 149-73-5
trimethyl orthoformate

: 476687-99-7
C₄₃H₆₀O₁₂

Guidance literature:: With camphor-10-sulfonic acid; In methanol; at 80 ℃;
DOI:10.1021/ol026804w

Reference yield:

: 452-51-7,13046-70-3,29780-54-9,36792-87-7,36792-88-8,113890-35-0,113890-38-3
D-2-deoxyribose

: 476687-99-7
C₄₃H₆₀O₁₂

Guidance literature:: Multi-step reaction with 31 steps

1.1: 90 percent / aq. HCl / CHCl₃ / 20 °C

2.1: CSA / CH₂Cl₂ / 20 °C

3.1: N-methylmorpholine / CH₂Cl₂ / 20 °C

4.1: 98 percent / MeI; NaHCO₃ / H₂O; acetonitrile / 20 °C

5.1: 95 percent / SmI₂ / methanol; tetrahydrofuran / 0 °C

6.1: 2,6-lutidine / CH₂Cl₂ / 0 °C

7.1: DIBAH / CH₂Cl₂ / 0 °C

8.1: 2,6-lutidine / CH₂Cl₂ / -78 °C

9.1: NaI / acetone / 60 °C

10.1: LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

10.2: 100 percent / SiO₂; H₂O

11.1: TBAF / tetrahydrofuran / 20 °C

12.1: N-methylmorpholine / CH₂Cl₂ / 20 °C

13.1: 84 percent / SmI₂ / methanol; tetrahydrofuran / 20 °C

14.1: 100 percent / DIBAH / toluene / -78 °C

15.1: 100 percent / toluene / 100 °C

16.1: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0 °C

17.1: 89 percent / DIBAH / toluene / -78 °C

18.1: 96 percent / (-)-DET; Ti(OiPr)4; TBHP / 4 Angstroem MS / CH₂Cl₂ / -35 °C

19.1: SO₃*pyridine; Et₃N / dimethylsulfoxide; CH₂Cl₂ / 20 °C

20.1: NaHMDS / tetrahydrofuran / 0 °C

21.1: 74 percent / TBAF / tetrahydrofuran / 20 °C

22.1: 68 percent / PPTS / CH₂Cl₂ / 0 °C

23.1: 9-BBN / tetrahydrofuran / 0 °C

23.2: 82 percent / 30percent H₂O₂; 3 N NaOH / tetrahydrofuran / 0 °C

24.1: 87 percent / NaH; Bu₄NI / tetrahydrofuran / 0 °C

25.1: 85 percent / CSA / methanol / 20 °C

26.1: 2,6-lutidine / CH₂Cl₂ / -78 °C

26.2: 100 percent / CH₂Cl₂ / -78 °C

27.1: 100 percent / t-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

28.1: CSA / methanol / 20 °C

29.1: 2,6-lutidine / CH₂Cl₂ / 0 °C

30.1: 83 percent / NaIO₄ / RuO₂ / acetonitrile; CCl₄; H₂O / 20 °C

31.1: 67 percent / CSA / methanol / 80 °C

With 4-methyl-morpholine; 2,6-dimethylpyridine; titanium(IV) isopropylate; hydrogenchloride; tert.-butylhydroperoxide; sodium periodate; 9-borabicyclo[3.3.1]nonane dimer; samarium diiodide; pyridine-SO₃ complex; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; tert.-butyl lithium; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; (-)-diethyl tartrate; triethylamine; sodium iodide; lithium diisopropyl amide; methyl iodide; ruthenium(IV) oxide; 4 Angstroem MS; In tetrahydrofuran; methanol; tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; chloroform; water; dimethyl sulfoxide; acetone; toluene; acetonitrile; 3.1: hetero-Michael reaction / 12.1: hetero-Michael reaction / 15.1: Wittig reaction / 18.1: Sharpless epoxidation / 20.1: Wittig reaction;
DOI:10.1021/ol026804w

Reference yield:

: 50907-65-8
2-deoxy-D-erythro-pentose cyclic 1,3-propanediyl mercaptal

: 476687-99-7
C₄₃H₆₀O₁₂

Guidance literature:: Multi-step reaction with 30 steps

1.1: CSA / CH₂Cl₂ / 20 °C

2.1: N-methylmorpholine / CH₂Cl₂ / 20 °C

3.1: 98 percent / MeI; NaHCO₃ / H₂O; acetonitrile / 20 °C

4.1: 95 percent / SmI₂ / methanol; tetrahydrofuran / 0 °C

5.1: 2,6-lutidine / CH₂Cl₂ / 0 °C

6.1: DIBAH / CH₂Cl₂ / 0 °C

7.1: 2,6-lutidine / CH₂Cl₂ / -78 °C

8.1: NaI / acetone / 60 °C

9.1: LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

9.2: 100 percent / SiO₂; H₂O

10.1: TBAF / tetrahydrofuran / 20 °C

11.1: N-methylmorpholine / CH₂Cl₂ / 20 °C

12.1: 84 percent / SmI₂ / methanol; tetrahydrofuran / 20 °C

13.1: 100 percent / DIBAH / toluene / -78 °C

14.1: 100 percent / toluene / 100 °C

15.1: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0 °C

16.1: 89 percent / DIBAH / toluene / -78 °C

17.1: 96 percent / (-)-DET; Ti(OiPr)4; TBHP / 4 Angstroem MS / CH₂Cl₂ / -35 °C

18.1: SO₃*pyridine; Et₃N / dimethylsulfoxide; CH₂Cl₂ / 20 °C

19.1: NaHMDS / tetrahydrofuran / 0 °C

20.1: 74 percent / TBAF / tetrahydrofuran / 20 °C

21.1: 68 percent / PPTS / CH₂Cl₂ / 0 °C

22.1: 9-BBN / tetrahydrofuran / 0 °C

22.2: 82 percent / 30percent H₂O₂; 3 N NaOH / tetrahydrofuran / 0 °C

23.1: 87 percent / NaH; Bu₄NI / tetrahydrofuran / 0 °C

24.1: 85 percent / CSA / methanol / 20 °C

25.1: 2,6-lutidine / CH₂Cl₂ / -78 °C

25.2: 100 percent / CH₂Cl₂ / -78 °C

26.1: 100 percent / t-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 °C

27.1: CSA / methanol / 20 °C

28.1: 2,6-lutidine / CH₂Cl₂ / 0 °C

29.1: 83 percent / NaIO₄ / RuO₂ / acetonitrile; CCl₄; H₂O / 20 °C

30.1: 67 percent / CSA / methanol / 80 °C

With 4-methyl-morpholine; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium periodate; 9-borabicyclo[3.3.1]nonane dimer; samarium diiodide; pyridine-SO₃ complex; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; tert.-butyl lithium; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; (-)-diethyl tartrate; triethylamine; sodium iodide; lithium diisopropyl amide; methyl iodide; ruthenium(IV) oxide; 4 Angstroem MS; In tetrahydrofuran; methanol; tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; dimethyl sulfoxide; acetone; toluene; acetonitrile; 2.1: hetero-Michael reaction / 11.1: hetero-Michael reaction / 14.1: Wittig reaction / 17.1: Sharpless epoxidation / 19.1: Wittig reaction;
DOI:10.1021/ol026804w