2-O-acetyl-4-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6-O-trityl-β-D-glucopyranosylamine

Base Information

Chemical Name:2-O-acetyl-4-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6-O-trityl-β-D-glucopyranosylamine
CAS No.:193154-48-2
Molecular Formula:C₆₈H₆₉NO₁₁
Molecular Weight:1076.3
Hs Code.:

Synonyms:2-O-acetyl-4-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6-O-trityl-β-D-glucopyranosylamine

Suppliers and Price of 2-O-acetyl-4-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6-O-trityl-β-D-glucopyranosylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-O-acetyl-4-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6-O-trityl-β-D-glucopyranosylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-O-acetyl-4-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6-O-trityl-β-D-glucopyranosylamine

There total 6 articles about 2-O-acetyl-4-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6-O-trityl-β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (3aS,5R,6R,7S,7aR)-6-Benzyloxy-2-methyl-7-((2S,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-5-trityloxymethyl-5,6,7,7a-tetrahydro-3aH-pyrano[2,3-d]oxazole

: 193154-48-2
2-O-acetyl-4-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6-O-trityl-β-D-glucopyranosylamine

Guidance literature:: With sulfuric acid; In tetrahydrofuran; for 0.25h; Yield given;
DOI:10.1002/chem.19970030614

Reference yield:

: 122350-80-5
1,5-anhydro-2-deoxy-6-O-trityl-D-arabino-hex-1-enitol

: 193154-48-2
2-O-acetyl-4-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6-O-trityl-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) ZnCl₂, 2.) NaH / 1.) THF, 15 min, 2.) DMF, 2 h

2: 95 percent / 3,3-dimethyldioxirane / acetone; CH₂Cl₂ / 0.08 h / 0 °C

3: ZnCl₂ / tetrahydrofuran / 2 h

4: aq. H₂SO₄ / tetrahydrofuran / 0.25 h

With sulfuric acid; 3,3-dimethyldioxirane; sodium hydride; zinc(II) chloride; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1002/chem.19970030614

Reference yield:

: 100-39-0
benzyl bromide

: 193154-48-2
2-O-acetyl-4-O-benzyl-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-6-O-trityl-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) ZnCl₂, 2.) NaH / 1.) THF, 15 min, 2.) DMF, 2 h

2: 95 percent / 3,3-dimethyldioxirane / acetone; CH₂Cl₂ / 0.08 h / 0 °C

3: ZnCl₂ / tetrahydrofuran / 2 h

4: aq. H₂SO₄ / tetrahydrofuran / 0.25 h

With sulfuric acid; 3,3-dimethyldioxirane; sodium hydride; zinc(II) chloride; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1002/chem.19970030614