1,1-dimethylethyl 2-[(2-ethyl-4-{[(2-fluorophenyl)carbonyl]amino}phenyl)carbonyl]hydrazinecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl 2-[(2-ethyl-4-{[(2-fluorophenyl)carbonyl]amino}phenyl)carbonyl]hydrazinecarboxylate
CAS No.:959778-41-7
Molecular Formula:C₂₁H₂₄FN₃O₄
Molecular Weight:401.438
Hs Code.:

Synonyms:1,1-dimethylethyl 2-[(2-ethyl-4-{[(2-fluorophenyl)carbonyl]amino}phenyl)carbonyl]hydrazinecarboxylate

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Chemical Property of 1,1-dimethylethyl 2-[(2-ethyl-4-{[(2-fluorophenyl)carbonyl]amino}phenyl)carbonyl]hydrazinecarboxylate

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Technology Process of 1,1-dimethylethyl 2-[(2-ethyl-4-{[(2-fluorophenyl)carbonyl]amino}phenyl)carbonyl]hydrazinecarboxylate

There total 7 articles about 1,1-dimethylethyl 2-[(2-ethyl-4-{[(2-fluorophenyl)carbonyl]amino}phenyl)carbonyl]hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 959778-40-6
2-ethyl-4-{[(2-fluorophenyl)carbonyl]amino}benzoic acid

: 870-46-2
t-butoxycarbonylhydrazine

: 959778-41-7
1,1-dimethylethyl 2-[(2-ethyl-4-{[(2-fluorophenyl)carbonyl]amino}phenyl)carbonyl]hydrazinecarboxylate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 72h;

Reference yield:

: 959778-15-5
methyl 4-nitro-2-vinyl-benzoate

: 959778-41-7
1,1-dimethylethyl 2-[(2-ethyl-4-{[(2-fluorophenyl)carbonyl]amino}phenyl)carbonyl]hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / palladium 10% on activated carbon / methanol

2: triethylamine / dichloromethane / 2 h / 0 - 20 °C

3: sodium hydroxide; ethanol; water / 24 h / 20 - 60 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 72 h

With sodium hydroxide; ethanol; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium 10% on activated carbon; In methanol; dichloromethane;

Reference yield:

: 100959-22-6
methyl 2-bromo-4-nitrobenzoate

: 959778-41-7
1,1-dimethylethyl 2-[(2-ethyl-4-{[(2-fluorophenyl)carbonyl]amino}phenyl)carbonyl]hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; toluene / 2 h / 90 °C

2: hydrogen / palladium 10% on activated carbon / methanol

3: triethylamine / dichloromethane / 2 h / 0 - 20 °C

4: sodium hydroxide; ethanol; water / 24 h / 20 - 60 °C

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 72 h

With sodium hydroxide; ethanol; water; hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane; toluene;