(R,R)-trans-N,N’’-dimethyl-N,N’’-bis(2,6-difluoropyridin-4-yl)cyclohexane-1,2-diamine

Base Information

Chemical Name:(R,R)-trans-N,N’’-dimethyl-N,N’’-bis(2,6-difluoropyridin-4-yl)cyclohexane-1,2-diamine
CAS No.:1500084-25-2
Molecular Formula:C₁₈H₂₀F₄N₄
Molecular Weight:368.377
Hs Code.:

Synonyms:(R,R)-trans-N,N’’-dimethyl-N,N’’-bis(2,6-difluoropyridin-4-yl)cyclohexane-1,2-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,R)-trans-N,N’’-dimethyl-N,N’’-bis(2,6-difluoropyridin-4-yl)cyclohexane-1,2-diamine

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Technology Process of (R,R)-trans-N,N’’-dimethyl-N,N’’-bis(2,6-difluoropyridin-4-yl)cyclohexane-1,2-diamine

There total 1 articles about (R,R)-trans-N,N’’-dimethyl-N,N’’-bis(2,6-difluoropyridin-4-yl)cyclohexane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1500084-24-1
(R,R)-N,N’’-bis(2,6-difluoropyridin-4-yl)cyclohexane-1,2-diamine

: 74-88-4
methyl iodide

: 1500084-25-2
(R,R)-trans-N,N’’-dimethyl-N,N’’-bis(2,6-difluoropyridin-4-yl)cyclohexane-1,2-diamine

Guidance literature:: (R,R)-N,N’’-bis(2,6-difluoropyridin-4-yl)cyclohexane-1,2-diamine; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; mineral oil; for 48h;
DOI:10.1002/adsc.201500393

Reference yield: 95.0%

: 1500084-25-2
(R,R)-trans-N,N’’-dimethyl-N,N’’-bis(2,6-difluoropyridin-4-yl)cyclohexane-1,2-diamine

: 1500084-06-9
(R,R)-trans-N,N’-dimethyl-N,N’-bis(pyridin-4-yl)cyclohexane-1,2-diamine

Guidance literature:: With titanocene difluoride; diphenylsilane; In 1,4-dioxane; at 110 ℃; for 24h; Inert atmosphere;
DOI:10.1002/anie.201301927