C₂₂H₂₅NO₅S

Base Information

Chemical Name:C₂₂H₂₅NO₅S
CAS No.:1349706-16-6
Molecular Formula:C₂₂H₂₅NO₅S
Molecular Weight:415.51
Hs Code.:

C<sub>22</sub>H<sub>25</sub>NO<sub>5</sub>S

Synonyms:C₂₂H₂₅NO₅S

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Chemical Property of C₂₂H₂₅NO₅S

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Technology Process of C₂₂H₂₅NO₅S

There total 7 articles about C₂₂H₂₅NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1349705-88-9
C₂₂H₂₅NO₄S

: 1349706-16-6
C₂₂H₂₅NO₅S

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1039/c1ob06212c

Reference yield:

: 57476-50-3
1-tert-butoxycarbonyl-3-formylindole

: 1349706-16-6
C₂₂H₂₅NO₅S

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C

2: triethylamine / dichloromethane / 0.08 h / 20 °C

3: triethylamine / acetonitrile / 48 h / 20 °C

4: N,O-bis-(trimethylsilyl)-acetamide; potassium acetate / toluene / 0.07 h / 150 °C / Microwave irradiation

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 20 °C

With sodium tetrahydroborate; N,O-bis-(trimethylsilyl)-acetamide; potassium acetate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; toluene; acetonitrile; 4: Claisen rearrangement;
DOI:10.1039/c1ob06212c

Reference yield:

: 1349705-60-7
tert-butyl 3-((2-chloroacetoxy)methyl)-1H-indole-1-carboxylate

: 1349706-16-6
C₂₂H₂₅NO₅S

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / acetonitrile / 48 h / 20 °C

2: N,O-bis-(trimethylsilyl)-acetamide; potassium acetate / toluene / 0.07 h / 150 °C / Microwave irradiation

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 20 °C

With N,O-bis-(trimethylsilyl)-acetamide; potassium acetate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene; acetonitrile; 2: Claisen rearrangement;
DOI:10.1039/c1ob06212c