(E)-N-methyliminodiacetyl (1,1-dibromo-5-phenylpent-1-en-3-yl)boronate

Base Information

Chemical Name:(E)-N-methyliminodiacetyl (1,1-dibromo-5-phenylpent-1-en-3-yl)boronate
CAS No.:1329422-65-2
Molecular Formula:C₁₆H₁₈BBr₂NO₄
Molecular Weight:458.942
Hs Code.:

Synonyms:(E)-N-methyliminodiacetyl (1,1-dibromo-5-phenylpent-1-en-3-yl)boronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-methyliminodiacetyl (1,1-dibromo-5-phenylpent-1-en-3-yl)boronate

Chemical Property:

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Technology Process of (E)-N-methyliminodiacetyl (1,1-dibromo-5-phenylpent-1-en-3-yl)boronate

There total 3 articles about (E)-N-methyliminodiacetyl (1,1-dibromo-5-phenylpent-1-en-3-yl)boronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 558-13-4
carbon tetrabromide

: 1329422-58-3
N-methyliminodiacetyl (1-oxo-4-phenylbutan-2-yl)boronate

: 1329422-65-2
(E)-N-methyliminodiacetyl (1,1-dibromo-5-phenylpent-1-en-3-yl)boronate

Guidance literature:: With triphenylphosphine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ja205910d

Reference yield:

: N-methyliminodiacetyl (trans-3-phenethyloxiran-2-yl)boronate

: 1329422-65-2
(E)-N-methyliminodiacetyl (1,1-dibromo-5-phenylpent-1-en-3-yl)boronate

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / -30 - 0 °C

2: triphenylphosphine / dichloromethane / 0 - 20 °C

With boron trifluoride diethyl etherate; triphenylphosphine; In dichloromethane;
DOI:10.1021/ja205910d

Reference yield:

: (E)-6-methyl-2-(4-phenylbut-1-en-1-yl)-1,3,6,2-dioxazaborocane-4,8-dione

: 1329422-65-2
(E)-N-methyliminodiacetyl (1,1-dibromo-5-phenylpent-1-en-3-yl)boronate

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

2: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / -30 - 0 °C

3: triphenylphosphine / dichloromethane / 0 - 20 °C

With boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In dichloromethane;
DOI:10.1021/ja205910d