N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide

Base Information

Chemical Name:N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide
CAS No.:116005-70-0
Molecular Formula:C₂₀H₃₀N₄O₅
Molecular Weight:406.482
Hs Code.:

Synonyms:N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide

Suppliers and Price of N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide

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Technology Process of N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide

There total 1 articles about N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1668-10-6
glycinamide hydrochloride

: 94193-38-1
N-Cyclohexyl-N-methyl-4-(3-formyl-4-nitrophenyl)-oxybutyramide

: 116005-70-0
N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide

Guidance literature:: With sodium acetate; sodium cyanoborohydride; 1.) methanol, reflux, 2.) room temperature, 3 h;
DOI:10.1021/jm00119a015

Reference yield:

: 116005-70-0
N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide

: 116005-73-3
1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-aminobenzyl>hydantoin

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / Ambient temperature

2: 60 percent / sodium methoxide / methanol / 18 h / Heating

3: 65 percent / conc. HCl, hydrogen / Pd-C / ethanol / 1 h / 3102.9 Torr

With hydrogenchloride; hydrogen; sodium methylate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/jm00119a015

Reference yield:

: 116005-70-0
N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide

: 116005-74-4
N-cyclohexyl-N-methyl-4-<<3-(carbamoylmethyl)-1,2,3,4-tetrahydro-2-oxoquinazolin-6-yl>oxy>butyramide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 1 h / Ambient temperature

2: hydrogen / Pd-C / dimethylformamide / 3102.9 Torr

3: 24 percent / N,N-diisopropylethylamine, DMAP / tetrahydrofuran / Ambient temperature

With dmap; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00119a015