1-(3,5-cis-dimethylpiperidin-1-yl)-3-(4,6-dimethoxy-2-hydroxyphenyl)-3-(4-methylimidazol-4-yl)propan-1-one

Base Information

Chemical Name:1-(3,5-cis-dimethylpiperidin-1-yl)-3-(4,6-dimethoxy-2-hydroxyphenyl)-3-(4-methylimidazol-4-yl)propan-1-one
CAS No.:1427192-09-3
Molecular Formula:C₂₂H₃₁N₃O₄
Molecular Weight:401.506
Hs Code.:

Synonyms:1-(3,5-cis-dimethylpiperidin-1-yl)-3-(4,6-dimethoxy-2-hydroxyphenyl)-3-(4-methylimidazol-4-yl)propan-1-one

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Chemical Property of 1-(3,5-cis-dimethylpiperidin-1-yl)-3-(4,6-dimethoxy-2-hydroxyphenyl)-3-(4-methylimidazol-4-yl)propan-1-one

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Technology Process of 1-(3,5-cis-dimethylpiperidin-1-yl)-3-(4,6-dimethoxy-2-hydroxyphenyl)-3-(4-methylimidazol-4-yl)propan-1-one

There total 3 articles about 1-(3,5-cis-dimethylpiperidin-1-yl)-3-(4,6-dimethoxy-2-hydroxyphenyl)-3-(4-methylimidazol-4-yl)propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14446-75-4,32410-46-1,32452-46-3,35794-11-7
(3S,5R)-3,5-dimethylpiperidine

: 1427192-73-1
C₁₅H₁₆N₂O₄

: 1427192-09-3
1-(3,5-cis-dimethylpiperidin-1-yl)-3-(4,6-dimethoxy-2-hydroxyphenyl)-3-(4-methylimidazol-4-yl)propan-1-one

Guidance literature:: In tetrahydrofuran; at 60 ℃; for 12h;

Reference yield:

: 35034-22-1
2-methylimidazole-4⁽⁵⁾-carbaldehyde

: 1427192-09-3
1-(3,5-cis-dimethylpiperidin-1-yl)-3-(4,6-dimethoxy-2-hydroxyphenyl)-3-(4-methylimidazol-4-yl)propan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine / pyridine / 5 h / 100 °C / Inert atmosphere

2: trifluoroacetic acid / 1,2-dichloro-ethane / 0.75 h / 80 °C / Microwave irradiation

3: tetrahydrofuran / 12 h / 60 °C

With piperidine; trifluoroacetic acid; In tetrahydrofuran; pyridine; 1,2-dichloro-ethane;

Reference yield:

: 500-99-2
3,5-dimethoxyphenol

: 88874-23-1
2-methylurocanic acid

: 1427192-09-3
1-(3,5-cis-dimethylpiperidin-1-yl)-3-(4,6-dimethoxy-2-hydroxyphenyl)-3-(4-methylimidazol-4-yl)propan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 1,2-dichloro-ethane / 0.75 h / 80 °C / Microwave irradiation

2: tetrahydrofuran / 12 h / 60 °C

With trifluoroacetic acid; In tetrahydrofuran; 1,2-dichloro-ethane;