1-((E)-(4S,5S)-5-Methoxy-2,4-dimethyl-6-phenyl-hex-2-ene-1-sulfonyl)-4-methyl-benzene

Base Information

Chemical Name:1-((E)-(4S,5S)-5-Methoxy-2,4-dimethyl-6-phenyl-hex-2-ene-1-sulfonyl)-4-methyl-benzene
CAS No.:170872-80-7
Molecular Formula:C₂₂H₂₈O₃S
Molecular Weight:372.529
Hs Code.:

Synonyms:1-((E)-(4S,5S)-5-Methoxy-2,4-dimethyl-6-phenyl-hex-2-ene-1-sulfonyl)-4-methyl-benzene

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Chemical Property of 1-((E)-(4S,5S)-5-Methoxy-2,4-dimethyl-6-phenyl-hex-2-ene-1-sulfonyl)-4-methyl-benzene

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Technology Process of 1-((E)-(4S,5S)-5-Methoxy-2,4-dimethyl-6-phenyl-hex-2-ene-1-sulfonyl)-4-methyl-benzene

There total 2 articles about 1-((E)-(4S,5S)-5-Methoxy-2,4-dimethyl-6-phenyl-hex-2-ene-1-sulfonyl)-4-methyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126399-05-1
(2E,4S,5S)-5-methoxy-2,4-dimethyl-6-phenylhex-2-en-1-ol

: 170872-80-7
1-((E)-(4S,5S)-5-Methoxy-2,4-dimethyl-6-phenyl-hex-2-ene-1-sulfonyl)-4-methyl-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: (Bu₄N)Br, DME / Heating

With pyridine; 1,2-dimethoxyethane; tetrabutylammomium bromide;
DOI:10.1021/ja00140a025

Reference yield:

: 126399-04-0
(2E,4S,5S)-ethyl 5-methoxy-2,4-dimethyl-6-phenylhex-2-enoate

: 170872-80-7
1-((E)-(4S,5S)-5-Methoxy-2,4-dimethyl-6-phenyl-hex-2-ene-1-sulfonyl)-4-methyl-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / LiAlH₄

2: pyridine

3: (Bu₄N)Br, DME / Heating

With pyridine; lithium aluminium tetrahydride; 1,2-dimethoxyethane; tetrabutylammomium bromide;
DOI:10.1021/ja00140a025

Reference yield:

: 170872-80-7
1-((E)-(4S,5S)-5-Methoxy-2,4-dimethyl-6-phenyl-hex-2-ene-1-sulfonyl)-4-methyl-benzene

: 141672-08-4
(-)-motuporin

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) BuLi, 3.) sodium naphthalene, 4.) (COCl)2

2: 1.) LiOH, 2.) sodium naphthalene, 4.) DCC

3: diisopropylethylamine

4: Zn, HOAc

5: DCC

6: TFA / CH₂Cl₂

7: 52 percent / aq. Ba(OH)2

With barium dihydroxide; lithium hydroxide; n-butyllithium; oxalyl dichloride; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; sodium naphthalenide; trifluoroacetic acid; zinc; In dichloromethane;
DOI:10.1021/ja00140a025