[3-Hydroxymethyl-6,8-diisopropoxy-4-(4-isopropoxy-3-methoxy-phenyl)-naphthalen-2-yl]-(4-isopropoxy-3-methoxy-phenyl)-methanol

Base Information

Chemical Name:[3-Hydroxymethyl-6,8-diisopropoxy-4-(4-isopropoxy-3-methoxy-phenyl)-naphthalen-2-yl]-(4-isopropoxy-3-methoxy-phenyl)-methanol
CAS No.:133593-79-0
Molecular Formula:C₃₈H₄₈O₈
Molecular Weight:632.794
Hs Code.:

Synonyms:[3-Hydroxymethyl-6,8-diisopropoxy-4-(4-isopropoxy-3-methoxy-phenyl)-naphthalen-2-yl]-(4-isopropoxy-3-methoxy-phenyl)-methanol

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Chemical Property of [3-Hydroxymethyl-6,8-diisopropoxy-4-(4-isopropoxy-3-methoxy-phenyl)-naphthalen-2-yl]-(4-isopropoxy-3-methoxy-phenyl)-methanol

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Technology Process of [3-Hydroxymethyl-6,8-diisopropoxy-4-(4-isopropoxy-3-methoxy-phenyl)-naphthalen-2-yl]-(4-isopropoxy-3-methoxy-phenyl)-methanol

There total 25 articles about [3-Hydroxymethyl-6,8-diisopropoxy-4-(4-isopropoxy-3-methoxy-phenyl)-naphthalen-2-yl]-(4-isopropoxy-3-methoxy-phenyl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 133593-78-9
(+/-)-3,9-Bis(4-isopropoxy-3-methoxyphenyl)-5,7-diisopropoxynaphtho<2,3-c>furan-1(3H)-one

: 133593-79-0
[3-Hydroxymethyl-6,8-diisopropoxy-4-(4-isopropoxy-3-methoxy-phenyl)-naphthalen-2-yl]-(4-isopropoxy-3-methoxy-phenyl)-methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 25 ℃; for 2h;
DOI:10.1039/c39910000190

Reference yield: 40.0%

: 1516-60-5
4-nitrophenyl azide

: 754-05-2
ethenyltrimethylsilane

: 131991-97-4
1-(4-nitrophenyl)-2-(trimethylsilyl)aziridine

: 131991-93-0
4,5-Dihydro-1-(4-nitrophenyl)-4-(trimethylsilyl)-1,2,3-triazole

: 133593-79-0
[3-Hydroxymethyl-6,8-diisopropoxy-4-(4-isopropoxy-3-methoxy-phenyl)-naphthalen-2-yl]-(4-isopropoxy-3-methoxy-phenyl)-methanol

Guidance literature:: In neat (no solvent); at 70 ℃; for 5h;

Reference yield:

: 133593-69-8
6-Bromo-3-(hydroxymethyl)-5-methoxy-1-naphthol

: 133593-79-0
[3-Hydroxymethyl-6,8-diisopropoxy-4-(4-isopropoxy-3-methoxy-phenyl)-naphthalen-2-yl]-(4-isopropoxy-3-methoxy-phenyl)-methanol

Guidance literature:: Multi-step reaction with 8 steps

1: 82 percent / K₂CO₃ / toluene / 96 h

3: 95 percent / toluene / 12 h / Heating

4: 85 percent / aq. NaOH / methanol / 96 h / Heating

6: 88 percent / tetrahydrofuran / 0.5 h / Ambient temperature

8: 99 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

With sodium hydroxide; lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; toluene;