pivaloyloxymethyl (2S)-2-N-[4-(N-benzyloxycarbonyl-N-methyl)aminobenzoyl]amino-4-(phenylselenyl)butyrate

Base Information

Chemical Name:pivaloyloxymethyl (2S)-2-N-[4-(N-benzyloxycarbonyl-N-methyl)aminobenzoyl]amino-4-(phenylselenyl)butyrate
CAS No.:875668-21-6
Molecular Formula:C₃₂H₃₆N₂O₇Se
Molecular Weight:639.607
Hs Code.:

Synonyms:pivaloyloxymethyl (2S)-2-N-[4-(N-benzyloxycarbonyl-N-methyl)aminobenzoyl]amino-4-(phenylselenyl)butyrate

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Chemical Property of pivaloyloxymethyl (2S)-2-N-[4-(N-benzyloxycarbonyl-N-methyl)aminobenzoyl]amino-4-(phenylselenyl)butyrate

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Technology Process of pivaloyloxymethyl (2S)-2-N-[4-(N-benzyloxycarbonyl-N-methyl)aminobenzoyl]amino-4-(phenylselenyl)butyrate

There total 3 articles about pivaloyloxymethyl (2S)-2-N-[4-(N-benzyloxycarbonyl-N-methyl)aminobenzoyl]amino-4-(phenylselenyl)butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 875668-20-5
(2S)-2-N-[4-(N-benzyloxycarbonyl-N-methyl)aminobenzoyl]amino-4-(phenylselenyl)butyric acid

: 53064-79-2
iodomethyl pivaloate

: 875668-21-6
pivaloyloxymethyl (2S)-2-N-[4-(N-benzyloxycarbonyl-N-methyl)aminobenzoyl]amino-4-(phenylselenyl)butyrate

Guidance literature:: With silver carbonate; dimethyl methane phosphonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jm050871p

Reference yield:

: 875668-08-9
methyl (2S)-4-bromo-2-N-[4-(N-benzyloxycarbonyl-N-methyl)aminobenzoyl]aminobutyrate

: 875668-21-6
pivaloyloxymethyl (2S)-2-N-[4-(N-benzyloxycarbonyl-N-methyl)aminobenzoyl]amino-4-(phenylselenyl)butyrate

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaBH₄ / ethanol

1.2: 90 percent / ethanol / 0.5 h

2.1: aq. LiOH / methanol; CH₂Cl₂ / 2 h / 20 °C

3.1: 276 mg / dimethyl methylphosphonate; Ag₂CO₃ / dimethylformamide / 20 °C

With lithium hydroxide; sodium tetrahydroborate; silver carbonate; dimethyl methane phosphonate; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050871p

Reference yield:

: 875668-19-2
methyl (2S)-2-N-[4-(N-carbobenzyloxy-N-methyl)aminobenzoyl]amino-4-(phenylselenyl)butyrate

: 875668-21-6
pivaloyloxymethyl (2S)-2-N-[4-(N-benzyloxycarbonyl-N-methyl)aminobenzoyl]amino-4-(phenylselenyl)butyrate

Guidance literature:: Multi-step reaction with 2 steps

1: aq. LiOH / methanol; CH₂Cl₂ / 2 h / 20 °C

2: 276 mg / dimethyl methylphosphonate; Ag₂CO₃ / dimethylformamide / 20 °C

With lithium hydroxide; silver carbonate; dimethyl methane phosphonate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm050871p