N-(4-(3-(4-(bis(2-chloroethyl)amino)phenyl)ureido)phenyl)-2-chloroacetamide

Base Information

Chemical Name:N-(4-(3-(4-(bis(2-chloroethyl)amino)phenyl)ureido)phenyl)-2-chloroacetamide
CAS No.:1586764-69-3
Molecular Formula:C₁₉H₂₁Cl₃N₄O₂
Molecular Weight:443.76
Hs Code.:

Synonyms:N-(4-(3-(4-(bis(2-chloroethyl)amino)phenyl)ureido)phenyl)-2-chloroacetamide

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Chemical Property of N-(4-(3-(4-(bis(2-chloroethyl)amino)phenyl)ureido)phenyl)-2-chloroacetamide

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Technology Process of N-(4-(3-(4-(bis(2-chloroethyl)amino)phenyl)ureido)phenyl)-2-chloroacetamide

There total 4 articles about N-(4-(3-(4-(bis(2-chloroethyl)amino)phenyl)ureido)phenyl)-2-chloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 17273-09-5
1-(4-aminophenyl)-3-(4-(bis(2-chloroethyl)amino)phenyl)urea

: 79-04-9
chloroacetyl chloride

: 1586764-69-3
N-(4-(3-(4-(bis(2-chloroethyl)amino)phenyl)ureido)phenyl)-2-chloroacetamide

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 0.75h;
DOI:10.1016/j.ejmech.2014.02.018

Reference yield:

: 2067-58-5
4-amino-N,N-bis(2-chloroethyl)aniline

: 1586764-69-3
N-(4-(3-(4-(bis(2-chloroethyl)amino)phenyl)ureido)phenyl)-2-chloroacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / chloroform / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 1551.49 - 1810.07 Torr

3: tetrahydrofuran / 0.75 h / 20 °C

With palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; chloroform; ethyl acetate;
DOI:10.1016/j.ejmech.2014.02.018

Reference yield:

: 100-28-7
4-Nitrophenyl isocyanate

: 1586764-69-3
N-(4-(3-(4-(bis(2-chloroethyl)amino)phenyl)ureido)phenyl)-2-chloroacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / chloroform / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 1551.49 - 1810.07 Torr

3: tetrahydrofuran / 0.75 h / 20 °C

With palladium 10% on activated carbon; hydrogen; triethylamine; In tetrahydrofuran; chloroform; ethyl acetate;
DOI:10.1016/j.ejmech.2014.02.018