(9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole-3,3'-diyl)bis(methylene) dibenzoate

Base Information

• Chemical Name: (9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole-3,3'-diyl)bis(methylene) dibenzoate
• CAS No.: 1312306-69-6
• Molecular Formula: C₄₀H₃₀N₄O₄
• Molecular Weight: 630.703

Synonyms:(9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole-3,3'-diyl)bis(methylene) dibenzoate

Chemical Property of (9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole-3,3'-diyl)bis(methylene) dibenzoate

Chemical Property:

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Technology Process of (9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole-3,3'-diyl)bis(methylene) dibenzoate

There total 2 articles about (9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole-3,3'-diyl)bis(methylene) dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(9,9'-dimethyl-9H,9'H-[1,1'-bipyrido[3,4-b]indole]-3,3'-diyl)dimethanol (1312306-67-4) + benzoyl chloride (98-88-4) → (9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole-3,3'-diyl)bis(methylene) dibenzoate (1312306-69-6)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1002/adsc.201100592

Reference yield:

dimethyl 9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole-3,3'-dicarboxylate (1312306-66-3) → (9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole-3,3'-diyl)bis(methylene) dibenzoate (1312306-69-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: 0 °C

2.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

With dmap; lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1002/adsc.201100592

Reference yield: 85.0%

(9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole-3,3'-diyl)bis(methylene) dibenzoate (1312306-69-6) → 3,3'-bis(benzoyloxymethyl)-9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole 2,2'-dioxide (1312426-14-4,1362679-98-8,1362680-02-1)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 24h;

DOI:10.1002/adsc.201100592

upstream raw materials:

dimethyl 9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole-3,3'-dicarboxylate

(9,9'-dimethyl-9H,9'H-[1,1'-bipyrido[3,4-b]indole]-3,3'-diyl)dimethanol

benzoyl chloride

Downstream raw materials:

3,3'-bis(benzoyloxymethyl)-9,9'-dimethyl-9H,9'H-1,1'-bipyrido[3,4-b]indole 2,2'-dioxide

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