1,3-bis{N^1'-[3'',4''-bis(benzyloxy)benzoyl]-N^4'-benzyloxycarbonylspermidinyl}-2-isopropyl citrate

Base Information

• Chemical Name: 1,3-bis{N^1'-[3'',4''-bis(benzyloxy)benzoyl]-N^4'-benzyloxycarbonylspermidinyl}-2-isopropyl citrate
• CAS No.: 1608483-50-6
• Molecular Formula: C₈₁H₉₂N₆O₁₅
• Molecular Weight: 1389.65

Synonyms:1,3-bis{N^1'-[3'',4''-bis(benzyloxy)benzoyl]-N^4'-benzyloxycarbonylspermidinyl}-2-isopropyl citrate

Chemical Property of 1,3-bis{N^1'-[3'',4''-bis(benzyloxy)benzoyl]-N^4'-benzyloxycarbonylspermidinyl}-2-isopropyl citrate

Chemical Property:

Purity/Quality:

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Technology Process of 1,3-bis{N^1'-[3'',4''-bis(benzyloxy)benzoyl]-N^4'-benzyloxycarbonylspermidinyl}-2-isopropyl citrate

There total 1 articles about 1,3-bis{N^1'-[3'',4''-bis(benzyloxy)benzoyl]-N^4'-benzyloxycarbonylspermidinyl}-2-isopropyl citrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

N1-[3,4-bis(benzyloxy)-benzoyl]-N4-benzyloxycarbonyl-spermidine trifluoroacetic acid + 2-isopropyl citrate (83966-25-0) → 1,3-bis{N1'-[3'',4''-bis(benzyloxy)benzoyl]-N4'-benzyloxycarbonylspermidinyl}-2-isopropyl citrate (1608483-50-6)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 18h; Molecular sieve; Inert atmosphere; Darkness;

DOI:10.1002/ejoc.201301340

Reference yield:

1,3-bis{N1'-[3'',4''-bis(benzyloxy)benzoyl]-N4'-benzyloxycarbonylspermidinyl}-2-isopropyl citrate (1608483-50-6) → C78H86N6O15 (1608483-55-1)

Guidance literature:

1,3-bis{N^1'-[3'',4''-bis(benzyloxy)benzoyl]-N^4'-benzyloxycarbonylspermidinyl}-2-isopropyl citrate; With lithium hydroxide; In tetrahydrofuran; water; at 0 ℃; for 0.666667h; Inert atmosphere; Darkness;

In tetrahydrofuran; water; for 0.166667h; Inert atmosphere;

DOI:10.1002/ejoc.201301340

Reference yield:

1,3-bis{N1'-[3'',4''-bis(benzyloxy)benzoyl]-N4'-benzyloxycarbonylspermidinyl}-2-isopropyl citrate (1608483-50-6) → C79H88N6O15

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 0 ℃; for 0.666667h; Inert atmosphere;

DOI:10.1002/ejoc.201301340

upstream raw materials:

2-isopropyl citrate

Downstream raw materials:

C₇₈H₈₆N₆O₁₅

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