1-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-3-(3-(methylamino)phenyl)urea

Base Information

• Chemical Name: 1-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-3-(3-(methylamino)phenyl)urea
• CAS No.: 1067199-39-6
• Molecular Formula: C₂₅H₂₈N₆O₄
• Molecular Weight: 476.535

Synonyms:1-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-3-(3-(methylamino)phenyl)urea

Chemical Property of 1-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-3-(3-(methylamino)phenyl)urea

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Technology Process of 1-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-3-(3-(methylamino)phenyl)urea

There total 2 articles about 1-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-3-(3-(methylamino)phenyl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate (1067199-34-1) → 1-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-3-(3-(methylamino)phenyl)urea (1067199-39-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1021/ja805758v

Reference yield: 85.0%

tert-butyl 3-(3-(3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethylureido)phenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate (1067199-37-4) → 1-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-3-(3-(methylamino)phenyl)urea (1067199-39-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1021/ja805758v

Reference yield: 94.0%

1-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-3-(3-(methylamino)phenyl)urea (1067199-39-6) + 4-nitrophenyl 3-(3-benzyl-3-phenylureido)phenylcarbamate (1067199-25-0) → 1-(3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-ureido)phenyl)-1-methyl-3-(3-(3-benzyl-3-phenylureido)phenyl)urea (1067199-44-3)

Guidance literature:

With dmap; In tetrahydrofuran; at 20 ℃; for 14h; Inert atmosphere;

DOI:10.1021/ja805758v

upstream raw materials:

3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate

tert-butyl 3-(3-(3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethylureido)phenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate

Downstream raw materials:

1-(3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-ureido)phenyl)-1-methyl-3-(3-(3-benzyl-3-phenylureido)phenyl)urea

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