3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate

Base Information

• Chemical Name: 3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate
• CAS No.: 1067199-34-1
• Molecular Formula: C₃₀H₃₆N₆O₆
• Molecular Weight: 576.652

Synonyms:3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate

Chemical Property of 3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate

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Technology Process of 3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate

There total 1 articles about 3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

tert-butyl 3-(3-(3-(3-(3-nitrophenyl)ureido)phenyl)-1,3-dimethylureido)phenyl methylcarbamate (1067199-33-0) + methyl iodide (74-88-4) → 3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate (1067199-34-1)

Guidance literature:

tert-butyl 3-(3-(3-(3-(3-nitrophenyl)ureido)phenyl)-1,3-dimethylureido)phenyl methylcarbamate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 10h;

DOI:10.1021/ja805758v

Reference yield: 98.0%

3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate (1067199-34-1) → tert-butyl 3-(3-(3-(3-(3-aminophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethyl carbamate (1067199-35-2)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; isopropyl alcohol; for 18h;

DOI:10.1021/ja805758v

Reference yield: 97.0%

3-(3-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethylcarbamate (1067199-34-1) → 1-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-3-(3-(methylamino)phenyl)urea (1067199-39-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere;

DOI:10.1021/ja805758v

upstream raw materials:

tert-butyl 3-(3-(3-(3-(3-nitrophenyl)ureido)phenyl)-1,3-dimethylureido)phenyl methylcarbamate

methyl iodide

Downstream raw materials:

tert-butyl 3-(3-(3-(3-(3-aminophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethylureido)phenylmethyl carbamate

1-(3-(3-(3-nitrophenyl)-1,3-dimethyl-ureido)phenyl)-1,3-dimethyl-3-(3-(methylamino)phenyl)urea

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