(E)-S-(2-diphenylthiophosphinyl-1-phenylethenyl) O-ethyl dithiocarbonate

Base Information

Chemical Name:(E)-S-(2-diphenylthiophosphinyl-1-phenylethenyl) O-ethyl dithiocarbonate
CAS No.:1134374-01-8
Molecular Formula:C₂₃H₂₁OPS₃
Molecular Weight:440.591
Hs Code.:

Synonyms:(E)-S-(2-diphenylthiophosphinyl-1-phenylethenyl) O-ethyl dithiocarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-S-(2-diphenylthiophosphinyl-1-phenylethenyl) O-ethyl dithiocarbonate

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Technology Process of (E)-S-(2-diphenylthiophosphinyl-1-phenylethenyl) O-ethyl dithiocarbonate

There total 1 articles about (E)-S-(2-diphenylthiophosphinyl-1-phenylethenyl) O-ethyl dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1134373-98-0
S-diphenylthiophosphinyl O-ethyl dithiocarbonate

: 536-74-3
phenylacetylene

: 1134374-01-8
(E)-S-(2-diphenylthiophosphinyl-1-phenylethenyl) O-ethyl dithiocarbonate

Guidance literature:: With dilauryl peroxide; In benzene; for 4h; stereoselective reaction; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2008.12.071

Reference yield: 98.0%

: 1134374-01-8
(E)-S-(2-diphenylthiophosphinyl-1-phenylethenyl) O-ethyl dithiocarbonate

: 106-95-6
allyl bromide

: 1134374-50-7
(E)-{1-allylthio-2-(diphenylthiophosphinyl)ethenyl}benzene

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 0.5h; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2008.12.071

Reference yield: 98.0%

: 1134374-01-8
(E)-S-(2-diphenylthiophosphinyl-1-phenylethenyl) O-ethyl dithiocarbonate

: 74-88-4
methyl iodide

: 1134374-05-2
(E)-{2-diphenylthiophosphinyl-1-(methylthio)ethenyl}benzene

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 0.5h; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2008.12.071