2-bromo-6-chloro-4-cyanophenyl acetate

Base Information

Chemical Name:2-bromo-6-chloro-4-cyanophenyl acetate
CAS No.:1689-87-8
Molecular Formula:C₉H₅BrClNO₂
Molecular Weight:274.501
Hs Code.:

Synonyms:2-bromo-6-chloro-4-cyanophenyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-6-chloro-4-cyanophenyl acetate

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Technology Process of 2-bromo-6-chloro-4-cyanophenyl acetate

There total 1 articles about 2-bromo-6-chloro-4-cyanophenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1689-86-7
5-bromo-3-chloro-4-hydroxybenzonitrile

: 108-24-7
acetic anhydride

: 1689-87-8
2-bromo-6-chloro-4-cyanophenyl acetate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/acsinfecdis.7b00218

Reference yield:

: 3739-64-8
allyl n-butyl ether

: 1689-87-8
2-bromo-6-chloro-4-cyanophenyl acetate

: 1689-86-7
5-bromo-3-chloro-4-hydroxybenzonitrile

: 3-(3-butoxypropyl)-5-chloro-4-hydroxybenzonitrile

Guidance literature:: allyl n-butyl ether; With borane-THF; In tetrahydrofuran; at 20 ℃; for 0.25h; Cooling with ice; Inert atmosphere;

2-bromo-6-chloro-4-cyanophenyl acetate; With potassium phosphate; palladium diacetate; ruphos; In tetrahydrofuran; water; toluene; for 16h; Sealed tube; Heating; Inert atmosphere;
DOI:10.1021/acsinfecdis.7b00218

Reference yield:

: 15193-19-8
4-pentenyl ethyl ether

: 1689-87-8
2-bromo-6-chloro-4-cyanophenyl acetate

: 1689-86-7
5-bromo-3-chloro-4-hydroxybenzonitrile

: 3-chloro-5-(5-ethoxypentyl)-4-hydroxybenzonitrile

Guidance literature:: 4-pentenyl ethyl ether; With borane-THF; In tetrahydrofuran; at 20 ℃; for 0.25h; Cooling with ice; Inert atmosphere;

2-bromo-6-chloro-4-cyanophenyl acetate; With potassium phosphate; palladium diacetate; ruphos; In tetrahydrofuran; water; toluene; for 16h; Sealed tube; Heating; Inert atmosphere;
DOI:10.1021/acsinfecdis.7b00218