2-Azabicyclo[2.1.1]hexane-1-methanamine,2-(1-methylethyl)-(9CI)

Base Information

Chemical Name:2-Azabicyclo[2.1.1]hexane-1-methanamine,2-(1-methylethyl)-(9CI)
CAS No.:463961-55-9
Molecular Formula:C9H18N2
Molecular Weight:154.25
Hs Code.:
Mol file:463961-55-9.mol

Synonyms:2-Azabicyclo[2.1.1]hexane-1-methanamine,2-(1-methylethyl)-(9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Azabicyclo[2.1.1]hexane-1-methanamine,2-(1-methylethyl)-(9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

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Technology Process of 2-Azabicyclo[2.1.1]hexane-1-methanamine,2-(1-methylethyl)-(9CI)

There total 4 articles about 2-Azabicyclo[2.1.1]hexane-1-methanamine,2-(1-methylethyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 463961-49-1
2-(1-methylethyl)-2-azabicyclo[2.1.1]hexane-1-carbonitrile

: 463961-55-9
(2-isopropyl-2-azabicyclo[2.1.1]hex-1-yl)methylamine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃;
DOI:10.1021/jo025897s

Reference yield:

: 175021-13-3
3-(chloromethyl)cyclobutan-1-one

: 463961-55-9
(2-isopropyl-2-azabicyclo[2.1.1]hex-1-yl)methylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / titanium(IV) chloride / diethyl ether / 20 °C

2: 68 percent / methanol / 120 h

3: 78 percent / LiAlH₄ / diethyl ether / 20 °C

With lithium aluminium tetrahydride; titanium tetrachloride; In methanol; diethyl ether;
DOI:10.1021/jo025897s

Reference yield:

: 175021-14-4
N-<3-(chloromethyl)-1-cyclobutylidene>isopropylamine

: 463961-55-9
(2-isopropyl-2-azabicyclo[2.1.1]hex-1-yl)methylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / methanol / 120 h

2: 78 percent / LiAlH₄ / diethyl ether / 20 °C

With lithium aluminium tetrahydride; In methanol; diethyl ether;
DOI:10.1021/jo025897s