(22E)-22,23-dehydrocholesterol benzoate

Base Information

Chemical Name:(22E)-22,23-dehydrocholesterol benzoate
CAS No.:64110-88-9
Molecular Formula:C₃₄H₄₈O₂
Molecular Weight:488.754
Hs Code.:

Synonyms:(22E)-22,23-dehydrocholesterol benzoate

Suppliers and Price of (22E)-22,23-dehydrocholesterol benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (22E)-22,23-dehydrocholesterol benzoate

Chemical Property:

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Technology Process of (22E)-22,23-dehydrocholesterol benzoate

There total 3 articles about (22E)-22,23-dehydrocholesterol benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 34347-28-9,136897-21-7,137760-64-6,70755-51-0,566-89-2
22-dehydrocholesterol

: 98-88-4
benzoyl chloride

: 64110-88-9
(22E)-22,23-dehydrocholesterol benzoate

Guidance literature:: With pyridine; at 0 ℃; for 1h;

Reference yield:

: 10211-88-8
(20S)-3β-acetoxybisnorchol-5-en-22-al

: 64110-88-9
(22E)-22,23-dehydrocholesterol benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: KOH; ethanol

With potassium hydroxide; diethyl ether; ethanol;
DOI:10.1021/jo01103a002