N⁶-benzoyl-5'-O-(4,4'-dimethoxytriphenyl)methyl-2'-O,4'-C-(N-methylaminomethylene)adenosine

Base Information

• Chemical Name: N⁶-benzoyl-5'-O-(4,4'-dimethoxytriphenyl)methyl-2'-O,4'-C-(N-methylaminomethylene)adenosine
• CAS No.: 1247023-36-4
• Molecular Formula: C₄₀H₃₈N₆O₇
• Molecular Weight: 714.778

Synonyms:N⁶-benzoyl-5'-O-(4,4'-dimethoxytriphenyl)methyl-2'-O,4'-C-(N-methylaminomethylene)adenosine

Chemical Property of N⁶-benzoyl-5'-O-(4,4'-dimethoxytriphenyl)methyl-2'-O,4'-C-(N-methylaminomethylene)adenosine

Chemical Property:

Purity/Quality:

99% ,98%,Electron Grade , ^*data from raw suppliers

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Technology Process of N⁶-benzoyl-5'-O-(4,4'-dimethoxytriphenyl)methyl-2'-O,4'-C-(N-methylaminomethylene)adenosine

There total 8 articles about N⁶-benzoyl-5'-O-(4,4'-dimethoxytriphenyl)methyl-2'-O,4'-C-(N-methylaminomethylene)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-N-benzoyl-2'-O,4'-C-(N-methylaminomethylene)adenosine (1247023-34-2) + 4,4'-dimethoxytrityl chloride (40615-36-9) → N6-benzoyl-5'-O-(4,4'-dimethoxytriphenyl)methyl-2'-O,4'-C-(N-methylaminomethylene)adenosine (1247023-36-4)

Guidance literature:

With pyridine; at 20 ℃; for 12h;

Reference yield:

N6-benzoyladenine (4005-49-6) → N6-benzoyl-5'-O-(4,4'-dimethoxytriphenyl)methyl-2'-O,4'-C-(N-methylaminomethylene)adenosine (1247023-36-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 0.67 h / 80 - 85 °C

1.2: 0.5 h

2.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 1.5 h / 20 °C

3.1: pyridine / 12 h / 20 °C

With pyridine; N,O-bis-(trimethylsilyl)-acetamide; triethylamine tris(hydrogen fluoride); triethylamine; In tetrahydrofuran; toluene;

Reference yield:

5-methyl-2'-O,4'-C-(N-methylaminomethylene)-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)uridine → N6-benzoyl-5'-O-(4,4'-dimethoxytriphenyl)methyl-2'-O,4'-C-(N-methylaminomethylene)adenosine (1247023-36-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 100 °C

1.2: 0.67 h / 100 °C

2.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 1.5 h / 20 °C

3.1: pyridine / 12 h / 20 °C

With pyridine; N,O-bis-(trimethylsilyl)-acetamide; triethylamine tris(hydrogen fluoride); triethylamine; In tetrahydrofuran; toluene;

upstream raw materials:

6-N-benzoyl-2'-O,4'-C-(N-methylaminomethylene)adenosine

4,4'-dimethoxytrityl chloride

N₆-benzoyladenine

N⁶-benzoyl-3',5'-O-(tetraisopropyldisiloxane)-2'-O,4'-C-(N-methylaminomethylene)adenosine

Downstream raw materials:

N⁶-benzoyl-3'-O-[2-cyanoethoxy(diisopropylamino)phosphino]-5'-O-(4,4'-dimethoxytriphenyl)methyl-2'-O,4'-C-(N-methylaminomethylene)adenosine

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