1-(azidomethyl)-2,4-difluorobenzene

Base Information

• Chemical Name: 1-(azidomethyl)-2,4-difluorobenzene
• CAS No.: 622372-75-2
• Molecular Formula: C₇H₅F₂N₃
• Molecular Weight: 169.134

Synonyms:1-(azidomethyl)-2,4-difluorobenzene

Chemical Property of 1-(azidomethyl)-2,4-difluorobenzene

Chemical Property:

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Technology Process of 1-(azidomethyl)-2,4-difluorobenzene

There total 6 articles about 1-(azidomethyl)-2,4-difluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1-(bromomethyl)-2,4-difluorobenzene (23915-07-3) → 1-(azidomethyl)-2,4-difluorobenzene (622372-75-2)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; for 6h; Heating;

DOI:10.1039/c9cc09216a

Reference yield: 93.0%

4-(chloromethyl)-1,2-difluorobenzene (698-80-6) → 1-(azidomethyl)-2,4-difluorobenzene (622372-75-2)

Guidance literature:

With sodium azide; potassium iodide; In water; acetone; at 20 ℃; for 60h; Inert atmosphere;

DOI:10.1002/anie.201612193

Reference yield:

2,4-difluorobenzyl chloride (452-07-3) → 1-(azidomethyl)-2,4-difluorobenzene (622372-75-2)

Guidance literature:

With sodium azide; In water; at 120 ℃; for 0.5h; Microwave irradiation;

upstream raw materials:

1-(bromomethyl)-2,4-difluorobenzene

2,4-difluorobenzyl chloride

4-(chloromethyl)-1,2-difluorobenzene

2,4-difluorobenzaldehyde

Downstream raw materials:

4-amino-N-((1-(2,4-difluorobenzyl)-1H-1,2,3-triazol-4-yl)methyl)benzenesulfonamide

(3S,4R,5R,6R)-4,5-bis((1-(2,4-difluorobenzyl)-1H-1,2,3-triazol-4-yl)methoxy)-2-(hydroxymethyl)-6-methoxy-tetra-hydro-2H-pyran-3-ol

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