1-[5-O-(4-methoxytrityl)-2-deoxy-2-phenylseleno-β-D-ribofuranosyl]uracil

Base Information

Chemical Name:1-[5-O-(4-methoxytrityl)-2-deoxy-2-phenylseleno-β-D-ribofuranosyl]uracil
CAS No.:133782-81-7
Molecular Formula:C₃₅H₃₂N₂O₆Se
Molecular Weight:655.609
Hs Code.:

Synonyms:1-[5-O-(4-methoxytrityl)-2-deoxy-2-phenylseleno-β-D-ribofuranosyl]uracil

Suppliers and Price of 1-[5-O-(4-methoxytrityl)-2-deoxy-2-phenylseleno-β-D-ribofuranosyl]uracil

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[5-O-(4-methoxytrityl)-2-deoxy-2-phenylseleno-β-D-ribofuranosyl]uracil

Chemical Property:

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Technology Process of 1-[5-O-(4-methoxytrityl)-2-deoxy-2-phenylseleno-β-D-ribofuranosyl]uracil

There total 3 articles about 1-[5-O-(4-methoxytrityl)-2-deoxy-2-phenylseleno-β-D-ribofuranosyl]uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1666-13-3
diphenyl diselenide

: 38642-30-7
2,2'-anhydro-1-[5-O-(4-methoxytrityl)-β-D-arabinofuranosyl]uracil

: 133782-81-7
1-[5-O-(4-methoxytrityl)-2-deoxy-2-phenylseleno-β-D-ribofuranosyl]uracil

Guidance literature:: diphenyl diselenide; With sodium tetrahydroborate; In tetrahydrofuran; ethanol; for 0.5h; Heating;

2,2'-anhydro-1-[5-O-(4-methoxytrityl)-β-D-arabinofuranosyl]uracil; In tetrahydrofuran; ethanol; for 1h; Further stages.; Heating;
DOI:10.1021/jo000967l

Reference yield:

: 3736-77-4
2,2'-Anhydrouridine

: 133782-81-7
1-[5-O-(4-methoxytrityl)-2-deoxy-2-phenylseleno-β-D-ribofuranosyl]uracil

Guidance literature:: Multi-step reaction with 2 steps

1.1: 82 percent / pyridine / 94 h / 20 °C

2.1: NaBH₄ / ethanol; tetrahydrofuran / 0.5 h / Heating

2.2: 90 percent / ethanol; tetrahydrofuran / 1 h / Heating

With pyridine; sodium tetrahydroborate; In tetrahydrofuran; ethanol;
DOI:10.1021/jo000967l

Reference yield:

: 14470-28-1
mono-4-methoxytrityl chloride

: 133782-81-7
1-[5-O-(4-methoxytrityl)-2-deoxy-2-phenylseleno-β-D-ribofuranosyl]uracil

Guidance literature:: Multi-step reaction with 2 steps

1.1: 82 percent / pyridine / 94 h / 20 °C

2.1: NaBH₄ / ethanol; tetrahydrofuran / 0.5 h / Heating

2.2: 90 percent / ethanol; tetrahydrofuran / 1 h / Heating

With pyridine; sodium tetrahydroborate; In tetrahydrofuran; ethanol;
DOI:10.1021/jo000967l