ethyl decachlorobenzilate

Base Information

Chemical Name:ethyl decachlorobenzilate
CAS No.:141709-01-5
Molecular Formula:C₁₆H₆Cl₁₀O₃
Molecular Weight:600.752
Hs Code.:

Synonyms:ethyl decachlorobenzilate

Suppliers and Price of ethyl decachlorobenzilate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl decachlorobenzilate

Chemical Property:

Purity/Quality:

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Technology Process of ethyl decachlorobenzilate

There total 1 articles about ethyl decachlorobenzilate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118-74-1,67471-27-6
hexachlorobenzene

: 95-92-1
oxalic acid diethyl ester

: 141709-01-5
ethyl decachlorobenzilate

Guidance literature:: With magnesium; ethylene dibromide; Yield given. Multistep reaction; 1) THF, 2) RT, 1 h;
DOI:10.1021/jo00042a021

Reference yield: 83.0%

: 141709-01-5
ethyl decachlorobenzilate

: 141725-93-1
ethyl bis(pentachlorophenyl)acetate

Guidance literature:: With phosphorus tribromide; In diethylene glycol dimethyl ether; Heating;
DOI:10.1021/jo00042a021

Reference yield:

: 141709-01-5
ethyl decachlorobenzilate

: 107846-89-9
bis(pentachlorophenyl)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / PBr₃ / bis-(2-methoxy-ethyl) ether / Heating

2: H₂SO₄ / 120 °C

With sulfuric acid; phosphorus tribromide; In diethylene glycol dimethyl ether;
DOI:10.1021/jo00042a021