3-[(2-tert-Butoxycarbonyl-ethyl)-trityl-amino]-propionic acid tert-butyl ester

Base Information

Chemical Name:3-[(2-tert-Butoxycarbonyl-ethyl)-trityl-amino]-propionic acid tert-butyl ester
CAS No.:146743-76-2
Molecular Formula:C₃₃H₄₁NO₄
Molecular Weight:515.693
Hs Code.:

Synonyms:3-[(2-tert-Butoxycarbonyl-ethyl)-trityl-amino]-propionic acid tert-butyl ester

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Chemical Property of 3-[(2-tert-Butoxycarbonyl-ethyl)-trityl-amino]-propionic acid tert-butyl ester

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Technology Process of 3-[(2-tert-Butoxycarbonyl-ethyl)-trityl-amino]-propionic acid tert-butyl ester

There total 2 articles about 3-[(2-tert-Butoxycarbonyl-ethyl)-trityl-amino]-propionic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 76-83-5
trityl chloride

: 128988-04-5
di-tert-butyl 3,3’-azanediyldipropanoate

: 146743-76-2
3-[(2-tert-Butoxycarbonyl-ethyl)-trityl-amino]-propionic acid tert-butyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 18h;
DOI:10.3987/COM-92-6164

Reference yield:

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 146743-76-2
3-[(2-tert-Butoxycarbonyl-ethyl)-trityl-amino]-propionic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ / 96 h / 50 °C

2: 95 percent / Et₃N / CH₂Cl₂ / 18 h / 25 °C

With ammonia; triethylamine; In dichloromethane;
DOI:10.3987/COM-92-6164

Reference yield:

: 146743-76-2
3-[(2-tert-Butoxycarbonyl-ethyl)-trityl-amino]-propionic acid tert-butyl ester

: 54903-50-3
4,5,6,7-tetrahydrothieno[3,2-c]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: tert-BuOK / toluene / 0.75 h / 75 °C

2: 2-methyl-propan-2-ol / 1 h / 40 °C

3: 1.) HCOOH, 2.) O₃, CF₃COOH, 3.) Me₂S, 4.) H₂S(g), HCl(g), TiCl₄

With hydrogenchloride; formic acid; dimethylsulfide; hydrogen sulfide; potassium tert-butylate; titanium tetrachloride; ozone; trifluoroacetic acid; In toluene; tert-butyl alcohol;
DOI:10.3987/COM-92-6164