1-(2-chlorophenyl)ethyl(3-methyl-5-(4-nitrophenyl)isoxazol-4-yl)carbamate

Base Information

Chemical Name:1-(2-chlorophenyl)ethyl(3-methyl-5-(4-nitrophenyl)isoxazol-4-yl)carbamate
CAS No.:355024-58-7
Molecular Formula:C₁₉H₁₆ClN₃O₅
Molecular Weight:401.806
Hs Code.:

Synonyms:1-(2-chlorophenyl)ethyl(3-methyl-5-(4-nitrophenyl)isoxazol-4-yl)carbamate

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Chemical Property of 1-(2-chlorophenyl)ethyl(3-methyl-5-(4-nitrophenyl)isoxazol-4-yl)carbamate

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Technology Process of 1-(2-chlorophenyl)ethyl(3-methyl-5-(4-nitrophenyl)isoxazol-4-yl)carbamate

There total 5 articles about 1-(2-chlorophenyl)ethyl(3-methyl-5-(4-nitrophenyl)isoxazol-4-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 13524-04-4
2'-chloro-sec-phenethyl alcohol

: 91135-88-5
3-methyl-5-(4-nitrophenyl)isoxazole-4-carboxylic acid

: 355024-58-7
1-(2-chlorophenyl)ethyl(3-methyl-5-(4-nitrophenyl)isoxazol-4-yl)carbamate

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In toluene; at 125 ℃; for 2h; Sealed tube;

Reference yield:

: 1391908-11-4
methyl 3-methyl-5-(4-nitrophenyl)isoxazole-4-carboxylate

: 355024-58-7
1-(2-chlorophenyl)ethyl(3-methyl-5-(4-nitrophenyl)isoxazol-4-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; lithium hydroxide / 1,4-dioxane / 20 °C

1.2: pH < 6

2.1: triethylamine; diphenyl phosphoryl azide / toluene / 2 h / 125 °C / Sealed tube

With diphenyl phosphoryl azide; water; triethylamine; lithium hydroxide; In 1,4-dioxane; toluene;

Reference yield:

: 85963-91-3
methyl 2-(4-nitrobenzoyl)-3-oxobutanoate

: 355024-58-7
1-(2-chlorophenyl)ethyl(3-methyl-5-(4-nitrophenyl)isoxazol-4-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine hydrochloride / acetic acid / 2 h / 115 °C

1.2: 20 °C

2.1: water; lithium hydroxide / 1,4-dioxane / 20 °C

2.2: pH < 6

3.1: triethylamine; diphenyl phosphoryl azide / toluene / 2 h / 125 °C / Sealed tube

With diphenyl phosphoryl azide; hydroxylamine hydrochloride; water; triethylamine; lithium hydroxide; In 1,4-dioxane; acetic acid; toluene;