O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-2,6-dideoxy-6-[(phenylmethyl)amino]-D-arabino-hexitol

Base Information

Chemical Name:O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-2,6-dideoxy-6-[(phenylmethyl)amino]-D-arabino-hexitol
CAS No.:760928-01-6
Molecular Formula:C₃₄H₅₃NO₁₄
Molecular Weight:699.793
Hs Code.:

O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-2,6-dideoxy-6-[(phenylmethyl)amino]-D-arabino-hexitol

Synonyms:O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-2,6-dideoxy-6-[(phenylmethyl)amino]-D-arabino-hexitol

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Chemical Property of O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-2,6-dideoxy-6-[(phenylmethyl)amino]-D-arabino-hexitol

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Technology Process of O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-2,6-dideoxy-6-[(phenylmethyl)amino]-D-arabino-hexitol

There total 3 articles about O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-2,6-dideoxy-6-[(phenylmethyl)amino]-D-arabino-hexitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 100-52-7
benzaldehyde

: 203794-60-9
O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-6-amino-1,5-anhydro-2,6-dideoxy-D-arabino-hexitol

: 760928-01-6
O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-2,6-dideoxy-6-[(phenylmethyl)amino]-D-arabino-hexitol

: O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-6-[bis(phenylmethyl)amino]-2,6-dideoxy-D-arabino-hexitol

Guidance literature:: With borane pyridine; 4 A molecular sieve; In methanol; water; for 20h;
DOI:10.1002/1522-2675(20001108)83:11<2893::AID-HLCA2893>3.0.CO;2-G

Reference yield:

: 322761-79-5
O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-2,3,4-tri-O-(phenylmethyl)-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-6-azido-2,6-dideoxy-D-arabino-hexitol

: 760928-01-6
O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-2,6-dideoxy-6-[(phenylmethyl)amino]-D-arabino-hexitol

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / H₂ / 10 percent Pd/C / dioxane; H₂O / 20 h

2: 14 percent / 4 Angstroem mol. sieves; borane-pyridine complex / methanol; H₂O / 20 h

With borane pyridine; 4 A molecular sieve; hydrogen; palladium on activated charcoal; In 1,4-dioxane; methanol; water;
DOI:10.1002/1522-2675(20001108)83:11<2893::AID-HLCA2893>3.0.CO;2-G

Reference yield:

: 322761-86-4
O-3-O-{2,4,6-tri-O-benzoyl-3-O-[(1S)-1-cyclohexylmethyl)-2-oxo-2-(phenylmethoxy)ethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-2,3,4-tris-O-(phenylmethyl)-α-L-galactopyranosyl-(1->4)]}-1,5-anhydro-6-azido-2,6-dideoxy-D-arabino-hexitol

: 760928-01-6
O-3-O-[(1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranosyl-(1->3)-O-[6-deoxy-α-L-galactopyranosyl-(1->4)]-1,5-anhydro-2,6-dideoxy-6-[(phenylmethyl)amino]-D-arabino-hexitol

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / LiOH*H₂O / methanol; H₂O / 20 h / 65 °C

2: 67 percent / H₂ / 10 percent Pd/C / dioxane; H₂O / 20 h

3: 14 percent / 4 Angstroem mol. sieves; borane-pyridine complex / methanol; H₂O / 20 h

With lithium hydroxide; borane pyridine; 4 A molecular sieve; hydrogen; palladium on activated charcoal; In 1,4-dioxane; methanol; water;
DOI:10.1002/1522-2675(20001108)83:11<2893::AID-HLCA2893>3.0.CO;2-G