3-(2,7-dichloro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-9,10-diphenyl-anthracene-2-carboxylic acid

Base Information

Chemical Name:3-(2,7-dichloro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-9,10-diphenyl-anthracene-2-carboxylic acid
CAS No.:245122-43-4
Molecular Formula:C₄₀H₂₂Cl₂O₅
Molecular Weight:653.518
Hs Code.:

3-(2,7-dichloro-6-hydroxy-3-oxo-3<i>H</i>-xanthen-9-yl)-9,10-diphenyl-anthracene-2-carboxylic acid

Synonyms:3-(2,7-dichloro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-9,10-diphenyl-anthracene-2-carboxylic acid

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Chemical Property of 3-(2,7-dichloro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-9,10-diphenyl-anthracene-2-carboxylic acid

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Technology Process of 3-(2,7-dichloro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-9,10-diphenyl-anthracene-2-carboxylic acid

There total 4 articles about 3-(2,7-dichloro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-9,10-diphenyl-anthracene-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 61415-62-1
9,10-diphenylanthracene-2,3-dicarboxylic anhydride

: 95-88-5
4-Chlororesorcinol

: 245122-43-4
3-(2,7-dichloro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-9,10-diphenyl-anthracene-2-carboxylic acid

Guidance literature:: With methanesulfonic acid; at 80 - 85 ℃;
DOI:10.1002/(SICI)1521-3773(19991004)38:19<2899::AID-ANIE2899>3.0.CO;2-M

Reference yield:

: 61415-63-2
9,10-diphenyl-2,3-dimethoxycarbonyl anthracene

: 245122-43-4
3-(2,7-dichloro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-9,10-diphenyl-anthracene-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / KOH / dioxane; methanol / Heating

2: 97 percent / Ac₂O / Heating

3: 59 percent / CH₃SO₃H / 80 - 85 °C

With potassium hydroxide; methanesulfonic acid; acetic anhydride; In 1,4-dioxane; methanol; 1: Hydrolysis / 2: Dehydration / 3: Condensation;
DOI:10.1002/(SICI)1521-3773(19991004)38:19<2899::AID-ANIE2899>3.0.CO;2-M

Reference yield:

: 83687-12-1
C₃₀H₂₆O₆

: 245122-43-4
3-(2,7-dichloro-6-hydroxy-3-oxo-3H-xanthen-9-yl)-9,10-diphenyl-anthracene-2-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 41 percent / H₂SO₄ / CH₂Cl₂ / Heating

2: 91 percent / KOH / dioxane; methanol / Heating

3: 97 percent / Ac₂O / Heating

4: 59 percent / CH₃SO₃H / 80 - 85 °C

With potassium hydroxide; methanesulfonic acid; sulfuric acid; acetic anhydride; In 1,4-dioxane; methanol; dichloromethane; 1: Aromatisation / 2: Hydrolysis / 3: Dehydration / 4: Condensation;
DOI:10.1002/(SICI)1521-3773(19991004)38:19<2899::AID-ANIE2899>3.0.CO;2-M