C₂₄H₃₃BFN₃O₄

Base Information

Chemical Name:C₂₄H₃₃BFN₃O₄
CAS No.:1560643-01-7
Molecular Formula:C₂₄H₃₃BFN₃O₄
Molecular Weight:457.353
Hs Code.:

C<sub>24</sub>H<sub>33</sub>BFN<sub>3</sub>O<sub>4</sub>

Synonyms:C₂₄H₃₃BFN₃O₄

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Chemical Property of C₂₄H₃₃BFN₃O₄

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Technology Process of C₂₄H₃₃BFN₃O₄

There total 6 articles about C₂₄H₃₃BFN₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1445591-84-3
C₁₈H₂₁BrFN₃O₂

: 73183-34-3
bis(pinacol)diborane

: 1560643-01-7
C₂₄H₃₃BFN₃O₄

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,2-dimethoxyethane; at 90 ℃; for 2h; Inert atmosphere;

Reference yield:

: 203866-16-4
1-tert-butyl 2-methyl (2S,4S)-4-fluoropyrrolidine-1,2-dicarboxylate

: 1560643-01-7
C₂₄H₃₃BFN₃O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hydroxide; water / tetrahydrofuran / 2 h / 0 - 20 °C

1.2: pH 5

2.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

3.1: ammonium acetate / toluene / 5 h / 110 °C

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; ammonium acetate; water; potassium acetate; triethylamine; lithium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; toluene;

Reference yield:

: 74844-91-0,114676-69-6,135042-17-0,227935-38-8,102195-79-9
(2S,4S)-N-tert-butoxycarbonyl-4-hydroxyproline methyl ester

: 1560643-01-7
C₂₄H₃₃BFN₃O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: diethylamino-sulfur trifluoride / dichloromethane / 21 h / -78 - 20 °C

2.1: lithium hydroxide; water / tetrahydrofuran / 2 h / 0 - 20 °C

2.2: pH 5

3.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

4.1: ammonium acetate / toluene / 5 h / 110 °C

5.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; diethylamino-sulfur trifluoride; ammonium acetate; water; potassium acetate; triethylamine; lithium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; toluene;