C₅₈H₆₇Cl₄N₅O₁₂

Base Information

Chemical Name:C₅₈H₆₇Cl₄N₅O₁₂
CAS No.:1424402-48-1
Molecular Formula:C₅₈H₆₇Cl₄N₅O₁₂
Molecular Weight:1168.01
Hs Code.:

C<sub>58</sub>H<sub>67</sub>Cl<sub>4</sub>N<sub>5</sub>O<sub>12</sub>

Synonyms:C₅₈H₆₇Cl₄N₅O₁₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₈H₆₇Cl₄N₅O₁₂

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Technology Process of C₅₈H₆₇Cl₄N₅O₁₂

There total 12 articles about C₅₈H₆₇Cl₄N₅O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1424402-38-9
C₂₈H₃₄N₄O₆

: 436143-87-2
(R)-3-(3-Chloro-4-methoxy-phenyl)-2-[(E)-(5S,6S)-6-((4R,5R)-2,2-dimethyl-5-phenyl-[1,3]dioxolan-4-yl)-5-hydroxy-hept-2-enoylamino]-propionic acid 2,2,2-trichloro-ethyl ester

: 1424402-48-1
C₅₈H₆₇Cl₄N₅O₁₂

Guidance literature:: With dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jm301346z

Reference yield:

: 1424402-27-6
(R)-5-azido-3-((S)-4-benzyl-2-oxooxazolidine-3-carbonyl)heptanoic acid

: 1424402-48-1
C₅₈H₆₇Cl₄N₅O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

2.1: 16 h / Reflux; Inert atmosphere

3.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 0.67 h / 0 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C / Inert atmosphere

5.1: sodium hydrogencarbonate / water; acetone / 4 h / 20 °C / Inert atmosphere

6.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

7.1: trifluoroacetic acid / dichloromethane / 3.5 h / 0 °C / Inert atmosphere

8.1: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With dmap; lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; dihydrogen peroxide; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1021/jm301346z

Reference yield:

: 203739-34-8
(S)-4-benzyl-3-(6-bromo-1-oxohexyl)-2-oxazolidinone

: 1424402-48-1
C₅₈H₆₇Cl₄N₅O₁₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium azide / water; acetone / 74 h / 20 °C / Reflux; Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

3.1: trifluoroacetic acid / tetrahydrofuran; dichloromethane / 16 h / 20 °C / Inert atmosphere

4.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

4.2: 1 h / 0 °C / Inert atmosphere

5.1: 16 h / Reflux; Inert atmosphere

6.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 0.67 h / 0 °C / Inert atmosphere

7.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C / Inert atmosphere

8.1: sodium hydrogencarbonate / water; acetone / 4 h / 20 °C / Inert atmosphere

9.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

10.1: trifluoroacetic acid / dichloromethane / 3.5 h / 0 °C / Inert atmosphere

11.1: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With dmap; sodium azide; lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; dihydrogen peroxide; sodium hexamethyldisilazane; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1021/jm301346z