2',3',5'-tri-O-benzoyladenosine 6-N-(O,O-bis(2-cyanoethyl)phosphoramidate)

Base Information

Chemical Name:2',3',5'-tri-O-benzoyladenosine 6-N-(O,O-bis(2-cyanoethyl)phosphoramidate)
CAS No.:154971-65-0
Molecular Formula:C₃₇H₃₂N₇O₁₀P
Molecular Weight:765.676
Hs Code.:

Synonyms:2',3',5'-tri-O-benzoyladenosine 6-N-(O,O-bis(2-cyanoethyl)phosphoramidate)

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Chemical Property of 2',3',5'-tri-O-benzoyladenosine 6-N-(O,O-bis(2-cyanoethyl)phosphoramidate)

Chemical Property:

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Technology Process of 2',3',5'-tri-O-benzoyladenosine 6-N-(O,O-bis(2-cyanoethyl)phosphoramidate)

There total 5 articles about 2',3',5'-tri-O-benzoyladenosine 6-N-(O,O-bis(2-cyanoethyl)phosphoramidate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₇H₃₂N₇O₉P

: 154971-65-0
2',3',5'-tri-O-benzoyladenosine 6-N-(O,O-bis(2-cyanoethyl)phosphoramidate)

Guidance literature:: With tert.-butylhydroperoxide; In dichloromethane; for 1h; Yield given; Ambient temperature;
DOI:10.1021/ja00101a011

Reference yield:

: 102690-88-0
bis(2-cyanoethyl) diisopropylamidophosphite

: 154971-65-0
2',3',5'-tri-O-benzoyladenosine 6-N-(O,O-bis(2-cyanoethyl)phosphoramidate)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrazole / acetonitrile / 2 h / Ambient temperature

2: t-BuOOH / 1 h / Ambient temperature

With 1H-tetrazole; tert.-butylhydroperoxide; In acetonitrile;
DOI:10.1080/07328319808004744

Reference yield:

: 51549-15-6
2',3',5'-tri-O-benzoyladenosine

: 154971-65-0
2',3',5'-tri-O-benzoyladenosine 6-N-(O,O-bis(2-cyanoethyl)phosphoramidate)

Guidance literature:: Multi-step reaction with 2 steps

1: tetrazole / acetonitrile / 2 h / Ambient temperature

2: t-BuOOH / 1 h / Ambient temperature

With 1H-tetrazole; tert.-butylhydroperoxide; In acetonitrile;
DOI:10.1080/07328319808004744