C₂₆H₂₄N₂O₃

Base Information

Chemical Name:C₂₆H₂₄N₂O₃
CAS No.:1197340-03-6
Molecular Formula:C₂₆H₂₄N₂O₃
Molecular Weight:412.488
Hs Code.:

C<sub>26</sub>H<sub>24</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₆H₂₄N₂O₃

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Chemical Property of C₂₆H₂₄N₂O₃

Chemical Property:

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Technology Process of C₂₆H₂₄N₂O₃

There total 5 articles about C₂₆H₂₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34035-06-8
4-hydroxy-5-phenyl-1⁽²⁾H-pyrazole-3-carboxylic acid ethyl ester

: 100-39-0
benzyl bromide

: 1197340-04-7
C₂₆H₂₄N₂O₃

: 1197340-03-6
C₂₆H₂₄N₂O₃

Guidance literature:: 4-hydroxy-5-phenyl-1⁽²⁾H-pyrazole-3-carboxylic acid ethyl ester; With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.166667h;

benzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 1.5h;

With water; ammonium chloride; In N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 718-08-1
ethyl 3-oxo-4-phenylbutyrate

: 1197340-03-6
C₂₆H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4-acetamidobenzenesulfonyl azide; triethylamine / dichloromethane / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

2.2: 0 °C

3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C

3.2: 1.5 h / 0 - 20 °C

With 4-acetamidobenzenesulfonyl azide; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 66696-84-2
5-(1-hydroxy-2-phenylethylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione

: 1197340-03-6
C₂₆H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4 h / Reflux

2.1: 4-acetamidobenzenesulfonyl azide; triethylamine / dichloromethane / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

3.2: 0 °C

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C

4.2: 1.5 h / 0 - 20 °C

With 4-acetamidobenzenesulfonyl azide; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; mineral oil;