C₃₀H₂₁N₃O₄

Base Information

• Chemical Name: C₃₀H₂₁N₃O₄
• CAS No.: 868697-60-3
• Molecular Formula: C₃₀H₂₁N₃O₄
• Molecular Weight: 487.514
• Mol file: 868697-60-3.mol

Synonyms:C₃₀H₂₁N₃O₄

Chemical Property of C₃₀H₂₁N₃O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₁N₃O₄

There total 9 articles about C₃₀H₂₁N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

C17H12ClNO3 (868697-59-0) + 2-(4-aminophenoxy)benzonitrile (30202-91-6) → C30H21N3O4 (868697-60-3)

Guidance literature:

In cyclohexanol; at 120 ℃;

Reference yield:

3-hydroxy-benzeneacetic acid, methyl ester (42058-59-3) → C30H21N3O4 (868697-60-3)

Guidance literature:

Multi-step reaction with 5 steps

1: ammonium hydroxide / water / 0 - 20 °C

2: potassium carbonate / DMF (N,N-dimethyl-formamide) / 20 °C

3: potassium tert-butylate / DMF (N,N-dimethyl-formamide) / 1 h / -10 - 20 °C

4: thionyl chloride / DMF (N,N-dimethyl-formamide); dichloromethane / 3 h / 20 °C

5: cyclohexanol / 120 °C

With thionyl chloride; potassium tert-butylate; potassium carbonate; ammonium hydroxide; In DMF (N,N-dimethyl-formamide); dichloromethane; water; cyclohexanol;

Reference yield:

salicylonitrile (611-20-1) → C30H21N3O4 (868697-60-3)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / DMF (N,N-dimethyl-formamide) / 90 °C

2: hydrogen / palladium / ethanol; ethyl acetate / 2.5 h

3: cyclohexanol / 120 °C

With hydrogen; potassium carbonate; palladium; In DMF (N,N-dimethyl-formamide); ethanol; ethyl acetate; cyclohexanol;

upstream raw materials:

C₁₇H₁₂ClNO₃

2-(4-aminophenoxy)benzonitrile

salicylonitrile

C₁₇H₁₃NO₄

Downstream raw materials:

C₃₁H₃₂N₃O₇P