10,13,16-tris(p-tolylsulfonyl)-1,25-bis<(2H-tetrahydropyran-2-yl)oxy>-10,13,16-triazapentaicosane

Base Information

Chemical Name:10,13,16-tris(p-tolylsulfonyl)-1,25-bis<(2H-tetrahydropyran-2-yl)oxy>-10,13,16-triazapentaicosane
CAS No.:106961-25-5
Molecular Formula:C₅₃H₈₃N₃O₁₀S₃
Molecular Weight:1018.45
Hs Code.:

Synonyms:10,13,16-tris(p-tolylsulfonyl)-1,25-bis<(2H-tetrahydropyran-2-yl)oxy>-10,13,16-triazapentaicosane

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Chemical Property of 10,13,16-tris(p-tolylsulfonyl)-1,25-bis<(2H-tetrahydropyran-2-yl)oxy>-10,13,16-triazapentaicosane

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Technology Process of 10,13,16-tris(p-tolylsulfonyl)-1,25-bis<(2H-tetrahydropyran-2-yl)oxy>-10,13,16-triazapentaicosane

There total 3 articles about 10,13,16-tris(p-tolylsulfonyl)-1,25-bis<(2H-tetrahydropyran-2-yl)oxy>-10,13,16-triazapentaicosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 106961-25-5
10,13,16-tris(p-tolylsulfonyl)-1,25-bis<(2H-tetrahydropyran-2-yl)oxy>-10,13,16-triazapentaicosane

Guidance literature:: Multi-step reaction with 3 steps

1: conc. HCl / tetrahydrofuran / 7 h / Ambient temperature

2: 98 percent / Et₃N / CH₂Cl₂ / 1.) -18 deg C, 20 min, 2.) RT, 2 h

3: 72 percent / dimethylformamide / 6 h / 95 °C

With triethylamine; hydrogenchloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19860690308

Reference yield:

: 3937-56-2
1,9-Nonanediol

: 106961-25-5
10,13,16-tris(p-tolylsulfonyl)-1,25-bis<(2H-tetrahydropyran-2-yl)oxy>-10,13,16-triazapentaicosane

Guidance literature:: Multi-step reaction with 3 steps

1: conc. HCl / tetrahydrofuran / 7 h / Ambient temperature

2: 98 percent / Et₃N / CH₂Cl₂ / 1.) -18 deg C, 20 min, 2.) RT, 2 h

3: 72 percent / dimethylformamide / 6 h / 95 °C

With triethylamine; hydrogenchloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19860690308

Reference yield:

: 98847-00-8
9-<(2H-tetrahydropyran-2-yl)oxy>nonan-1-ol

: 106961-25-5
10,13,16-tris(p-tolylsulfonyl)-1,25-bis<(2H-tetrahydropyran-2-yl)oxy>-10,13,16-triazapentaicosane

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / CH₂Cl₂ / 1.) -18 deg C, 20 min, 2.) RT, 2 h

2: 72 percent / dimethylformamide / 6 h / 95 °C

With triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19860690308