(E)-2-(4-chlorostyryl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

Base Information

Chemical Name:(E)-2-(4-chlorostyryl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine
CAS No.:1245706-92-6
Molecular Formula:C₁₈H₁₄BClN₂
Molecular Weight:304.587
Hs Code.:

Synonyms:(E)-2-(4-chlorostyryl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(4-chlorostyryl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

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Technology Process of (E)-2-(4-chlorostyryl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

There total 1 articles about (E)-2-(4-chlorostyryl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1073-67-2,24991-47-7
4-vinylbenzyl chloride

: 5656-71-3
2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

: 1245706-92-6
(E)-2-(4-chlorostyryl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

Guidance literature:: bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; In dioxane; under N2 atm.; mixt. of p-Cl-styrene, C10H9N2B and Rh complex in dioxanestirred at 60°C for 4 h;
DOI:10.1246/cl.2010.558

Reference yield: 87.0%

: 1245706-92-6
(E)-2-(4-chlorostyryl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

: 5720-05-8
4-methylphenylboronic acid

: 1147459-46-8
(E)-2-(2-(4'-methylbiphenyl-4-yl)vinyl)-2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

Guidance literature:: With CsF; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In dioxane; react. of C24H26B2N2O2 with p-tolyl bromide in presence of Pd complex with aq. NaOH;
DOI:10.1246/cl.2010.558