N,N',N'',N''',N'''',N''''',N'''''',N'''''''-octamethyl-1-[3-(2,6-diethylphenylureido)phenylureido]-3-[3-(2-bromophenylureido)phenylureido]benzene

Base Information

• Chemical Name: N,N',N'',N''',N'''',N''''',N'''''',N'''''''-octamethyl-1-[3-(2,6-diethylphenylureido)phenylureido]-3-[3-(2-bromophenylureido)phenylureido]benzene
• CAS No.: 935750-96-2
• Molecular Formula: C₄₆H₅₃BrN₈O₄
• Molecular Weight: 861.882

Synonyms:N,N',N'',N''',N'''',N''''',N'''''',N'''''''-octamethyl-1-[3-(2,6-diethylphenylureido)phenylureido]-3-[3-(2-bromophenylureido)phenylureido]benzene

Chemical Property of N,N',N'',N''',N'''',N''''',N'''''',N'''''''-octamethyl-1-[3-(2,6-diethylphenylureido)phenylureido]-3-[3-(2-bromophenylureido)phenylureido]benzene

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Technology Process of N,N',N'',N''',N'''',N''''',N'''''',N'''''''-octamethyl-1-[3-(2,6-diethylphenylureido)phenylureido]-3-[3-(2-bromophenylureido)phenylureido]benzene

There total 1 articles about N,N',N'',N''',N'''',N''''',N'''''',N'''''''-octamethyl-1-[3-(2,6-diethylphenylureido)phenylureido]-3-[3-(2-bromophenylureido)phenylureido]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C38H37BrN8O4 + methyl iodide (74-88-4) → N,N',N'',N''',N'''',N''''',N'''''',N'''''''-octamethyl-1-[3-(2,6-diethylphenylureido)phenylureido]-3-[3-(2-bromophenylureido)phenylureido]benzene (935750-96-2)

Guidance literature:

With sodium hydride; In tetrahydrofuran;

DOI:10.1021/jo061989w

Reference yield: 75.0%

N,N',N'',N''',N'''',N''''',N'''''',N'''''''-octamethyl-1-[3-(2,6-diethylphenylureido)phenylureido]-3-[3-(2-bromophenylureido)phenylureido]benzene (935750-96-2) + (1S,2R,5S)-2-isopropyl-5-methylcyclohexyl (R)-4-methylbenzenesulfinate (1517-82-4,13064-80-7,20752-45-8,50444-99-0,83060-18-8,83060-21-3,91796-57-5,98147-48-9,124819-73-4,132829-99-3,134929-63-8,91177-13-8) → 1-(3-(3-(2-((Ss)-p-tolylsulfinyl)phenyl)-1,3-dimethyl-ureido)phenyl)-1-methyl-3-(3-(3-(3-(3-(2,6-diethylphenyl)-1,3 dimethyl)ureido)phenyl)-1,3-dimethylureido)phenylurea

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at -90 - -10 ℃; for 6h; Inert atmosphere;

DOI:10.1021/ja805758v

upstream raw materials:

methyl iodide

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