N,N-bis[6-N,N-bis(3,4-dihydroxybenzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

Base Information

Chemical Name:N,N-bis[6-N,N-bis(3,4-dihydroxybenzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine
CAS No.:1221887-36-0
Molecular Formula:C₃₂H₂₈N₆O₆
Molecular Weight:592.611
Hs Code.:

Synonyms:N,N-bis[6-N,N-bis(3,4-dihydroxybenzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-bis[6-N,N-bis(3,4-dihydroxybenzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

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Technology Process of N,N-bis[6-N,N-bis(3,4-dihydroxybenzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

There total 1 articles about N,N-bis[6-N,N-bis(3,4-dihydroxybenzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1221887-35-9
N,N-bis[6-N,N-bis(3,4-bis(benzyloxy)benzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

: 1221887-36-0
N,N-bis[6-N,N-bis(3,4-dihydroxybenzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

Guidance literature:: With trimethylsilyl iodide; In acetonitrile; for 24h;
DOI:10.1021/ic902070q

Reference yield: 56.0%

: ammonium hexafluorophosphate

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 1221887-36-0
N,N-bis[6-N,N-bis(3,4-dihydroxybenzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

: 7732-18-5
water

: 75-05-8,26809-02-9
acetonitrile

: [RuCl(N,N-bis[6-N,N-bis(3,4-dihydroxybenzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine)]PF₆*CH₃CN*4water

Guidance literature:: In methanol; refluxing methanolic soln. of pyridine deriv. and ruthenium compd. for 24 h; filtration, evapn., dissolving in methanol, addn. of NH4PF6, concg., filtration, washing with CH3CN, drying, elem. anal.;
DOI:10.1021/ic902070q