N,N-bis[6-N,N-bis(3,4-bis(benzyloxy)benzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

Base Information

Chemical Name:N,N-bis[6-N,N-bis(3,4-bis(benzyloxy)benzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine
CAS No.:1221887-35-9
Molecular Formula:C₆₀H₅₂N₆O₆
Molecular Weight:953.109
Hs Code.:

Synonyms:N,N-bis[6-N,N-bis(3,4-bis(benzyloxy)benzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

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Chemical Property of N,N-bis[6-N,N-bis(3,4-bis(benzyloxy)benzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

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Technology Process of N,N-bis[6-N,N-bis(3,4-bis(benzyloxy)benzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

There total 1 articles about N,N-bis[6-N,N-bis(3,4-bis(benzyloxy)benzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: N,N-bis(6-amino-2-pyridylmethyl)-N-(2-pyridylmethyl)amine*nHCl

: 1486-54-0
3,4-dibenzyloxybenzoyl chloride

: 1221887-35-9
N,N-bis[6-N,N-bis(3,4-bis(benzyloxy)benzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

Guidance literature:: N,N-bis(6-amino-2-pyridylmethyl)-N-(2-pyridylmethyl)amine*nHCl; 3,4-dibenzyloxybenzoyl chloride; With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

With dmap; In tetrahydrofuran; for 14h; Reflux; Inert atmosphere;
DOI:10.1021/ic902070q

Reference yield: 85.0%

: 1221887-35-9
N,N-bis[6-N,N-bis(3,4-bis(benzyloxy)benzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

: 1221887-36-0
N,N-bis[6-N,N-bis(3,4-dihydroxybenzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

Guidance literature:: With trimethylsilyl iodide; In acetonitrile; for 24h;
DOI:10.1021/ic902070q

Reference yield: 58.0%

: sodium hexaflorophosphate

: 14898-67-0
ruthenium(III) chloride trihydrate

: 1221887-35-9
N,N-bis[6-N,N-bis(3,4-bis(benzyloxy)benzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine

: [RuCl(N,N-bis[6-N,N-bis(3,4-bis(benzyloxy)benzamide)-2-pyridylmethyl]-N-(2-pyridylmethyl)amine)]PF₆*1.5water

Guidance literature:: In ethanol; addn. of pyridine deriv. to refluxing ethanolic soln. of ruthenium compd., refluxing for 24 h, addn. of N2PF6; concg., isolation of ppt., washing with ethanol and diethyl ether, drying, elem. anal.;
DOI:10.1021/ic902070q