C₄₈H₃₃N₃

Base Information

Chemical Name:C₄₈H₃₃N₃
CAS No.:1338068-92-0
Molecular Formula:C₄₈H₃₃N₃
Molecular Weight:651.81
Hs Code.:

C<sub>48</sub>H<sub>33</sub>N<sub>3</sub>

Synonyms:C₄₈H₃₃N₃

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Chemical Property of C₄₈H₃₃N₃

Chemical Property:

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Technology Process of C₄₈H₃₃N₃

There total 6 articles about C₄₈H₃₃N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1338068-91-9
C₃₆H₂₃BrN₂

: 122-39-4
diphenylamine

: 1338068-92-0
C₄₈H₃₃N₃

Guidance literature:: With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; In toluene; at 80 ℃; for 4h; Inert atmosphere;

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 1338068-92-0
C₄₈H₃₃N₃

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate; copper; 18-crown-6 ether / 1,2-dichloro-benzene / 48 h / 170 - 180 °C

2: iodine; acetic acid; periodic acid / 2 h / 80 °C / Inert atmosphere

3: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 6 h / 90 °C / Inert atmosphere

4: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 6 h / 80 °C

5: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 4 h / 80 °C / Inert atmosphere

With 18-crown-6 ether; iodine; potassium acetate; copper; potassium carbonate; acetic acid; periodic acid; sodium t-butanolate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; In water; dimethyl sulfoxide; 1,2-dichloro-benzene; toluene;

Reference yield:

: 58328-30-6
5,11-diphenyl-5,11-dihydroindolo[3,2-b]carbazole

: 1338068-92-0
C₄₈H₃₃N₃

Guidance literature:: Multi-step reaction with 4 steps

1: iodine; acetic acid; periodic acid / 2 h / 80 °C / Inert atmosphere

2: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 6 h / 90 °C / Inert atmosphere

3: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 6 h / 80 °C

4: sodium t-butanolate / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 4 h / 80 °C / Inert atmosphere

With iodine; potassium acetate; potassium carbonate; acetic acid; periodic acid; sodium t-butanolate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; In water; dimethyl sulfoxide; toluene;