N-(1-tert-butyl-1H-imidazol-2-yl)-N'-(3,4-dichlorophenyl)guanidine hydrochloride

Base Information

Chemical Name:N-(1-tert-butyl-1H-imidazol-2-yl)-N'-(3,4-dichlorophenyl)guanidine hydrochloride
CAS No.:1404223-00-2
Molecular Formula:C₁₇H₁₅Cl₂N₅*ClH
Molecular Weight:396.707
Hs Code.:

Synonyms:N-(1-tert-butyl-1H-imidazol-2-yl)-N'-(3,4-dichlorophenyl)guanidine hydrochloride

Suppliers and Price of N-(1-tert-butyl-1H-imidazol-2-yl)-N'-(3,4-dichlorophenyl)guanidine hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(1-tert-butyl-1H-imidazol-2-yl)-N'-(3,4-dichlorophenyl)guanidine hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(1-tert-butyl-1H-imidazol-2-yl)-N'-(3,4-dichlorophenyl)guanidine hydrochloride

There total 4 articles about N-(1-tert-butyl-1H-imidazol-2-yl)-N'-(3,4-dichlorophenyl)guanidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1332704-17-2
1-(1-benzyl-1H-imidazol-2-yl)-3-(3,4-dichlorophenyl)thiourea

: 1404223-00-2
N-(1-tert-butyl-1H-imidazol-2-yl)-N'-(3,4-dichlorophenyl)guanidine hydrochloride

Guidance literature:: With ammonia; isobutyryl chloride; In methanol; N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/jm200503s

Reference yield:

: 100-46-9
benzylamine

: 1404223-00-2
N-(1-tert-butyl-1H-imidazol-2-yl)-N'-(3,4-dichlorophenyl)guanidine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: 18 h / 80 °C / Inert atmosphere; sealed tube

2.1: acetic acid / water / 1 h / 20 - 100 °C / Inert atmosphere

2.2: 0.25 h / 100 °C / Inert atmosphere

3.1: dichloromethane / 18 h / 20 °C / Inert atmosphere

4.1: ammonia; isobutyryl chloride / methanol; N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

With ammonia; acetic acid; isobutyryl chloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm200503s

Reference yield:

: 54879-88-8
N-benzyl-2,2-dimethoxyethylamine

: 1404223-00-2
N-(1-tert-butyl-1H-imidazol-2-yl)-N'-(3,4-dichlorophenyl)guanidine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / water / 1 h / 20 - 100 °C / Inert atmosphere

1.2: 0.25 h / 100 °C / Inert atmosphere

2.1: dichloromethane / 18 h / 20 °C / Inert atmosphere

3.1: ammonia; isobutyryl chloride / methanol; N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

With ammonia; acetic acid; isobutyryl chloride; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm200503s