1-[4-(1,4,7,10-tetraazacyclododecan-1-ylmethyl)benzyl]-1,4,8,11-tetraazacyclotetradecane

Base Information

Chemical Name:1-[4-(1,4,7,10-tetraazacyclododecan-1-ylmethyl)benzyl]-1,4,8,11-tetraazacyclotetradecane
CAS No.:613221-78-6
Molecular Formula:C₂₆H₅₀N₈
Molecular Weight:474.737
Hs Code.:

Synonyms:1-[4-(1,4,7,10-tetraazacyclododecan-1-ylmethyl)benzyl]-1,4,8,11-tetraazacyclotetradecane

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Chemical Property of 1-[4-(1,4,7,10-tetraazacyclododecan-1-ylmethyl)benzyl]-1,4,8,11-tetraazacyclotetradecane

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Technology Process of 1-[4-(1,4,7,10-tetraazacyclododecan-1-ylmethyl)benzyl]-1,4,8,11-tetraazacyclotetradecane

There total 6 articles about 1-[4-(1,4,7,10-tetraazacyclododecan-1-ylmethyl)benzyl]-1,4,8,11-tetraazacyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: C₃₀H₄₈N₈⁽²⁺⁾*2Br^(1-)

: 613221-78-6
1-[4-(1,4,7,10-tetraazacyclododecan-1-ylmethyl)benzyl]-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: With hydroxylamine hydrochloride; sodium ethanolate; In ethanol; for 4h; Heating;
DOI:10.1039/b103995b

Reference yield:

: (10bR,10cS)-3a-(4-Bromomethyl-benzyl)-decahydro-5a,8a,10a-triaza-3a-azonia-pyrene; bromide

: 613221-78-6
1-[4-(1,4,7,10-tetraazacyclododecan-1-ylmethyl)benzyl]-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / acetonitrile / 120 h / 20 °C

2: 92 percent / hydroxylamine hydrochloride; sodium ethoxide / ethanol / 4 h / Heating

With hydroxylamine hydrochloride; sodium ethanolate; In ethanol; acetonitrile;
DOI:10.1039/b103995b

Reference yield:

: 295-37-4
1,4,8,11-Tetraazacyclotetradecane

: 613221-78-6
1-[4-(1,4,7,10-tetraazacyclododecan-1-ylmethyl)benzyl]-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / H₂O; methanol / 3 h / 20 °C

2: 87 percent / tetrahydrofuran / 240 h / 20 °C

3: 86 percent / acetonitrile / 120 h / 20 °C

4: 92 percent / hydroxylamine hydrochloride; sodium ethoxide / ethanol / 4 h / Heating

With hydroxylamine hydrochloride; sodium ethanolate; In tetrahydrofuran; methanol; ethanol; water; acetonitrile;
DOI:10.1039/b103995b