(R)-[5-[2-[9-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]nonylamino]-1-hydroxyethyl]-2-phosphonooxybenzyl]-(diethyl)-[[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]carbonylmethyl]ammonium trifluoroacetate

Base Information

Chemical Name:(R)-[5-[2-[9-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]nonylamino]-1-hydroxyethyl]-2-phosphonooxybenzyl]-(diethyl)-[[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]carbonylmethyl]ammonium trifluoroacetate
CAS No.:1313485-83-4
Molecular Formula:C₂F₃O₂*C₇₀H₉₈N₄O₁₄P
Molecular Weight:1363.56
Hs Code.:

(R)-[5-[2-[9-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]nonylamino]-1-hydroxyethyl]-2-phosphonooxybenzyl]-(diethyl)-[[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]carbonylmethyl]ammonium trifluoroacetate

Synonyms:(R)-[5-[2-[9-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]nonylamino]-1-hydroxyethyl]-2-phosphonooxybenzyl]-(diethyl)-[[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]carbonylmethyl]ammonium trifluoroacetate

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Chemical Property of (R)-[5-[2-[9-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]nonylamino]-1-hydroxyethyl]-2-phosphonooxybenzyl]-(diethyl)-[[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]carbonylmethyl]ammonium trifluoroacetate

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Technology Process of (R)-[5-[2-[9-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]nonylamino]-1-hydroxyethyl]-2-phosphonooxybenzyl]-(diethyl)-[[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]carbonylmethyl]ammonium trifluoroacetate

There total 1 articles about (R)-[5-[2-[9-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]nonylamino]-1-hydroxyethyl]-2-phosphonooxybenzyl]-(diethyl)-[[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]carbonylmethyl]ammonium trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1200406-33-2
4-diethylaminoacetic acid [[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]] ester

: 1313485-94-7
(R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate

: 76-05-1
trifluoroacetic acid

: 1313485-83-4
(R)-[5-[2-[9-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]nonylamino]-1-hydroxyethyl]-2-phosphonooxybenzyl]-(diethyl)-[[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]carbonylmethyl]ammonium trifluoroacetate

Guidance literature:: (R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate; With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 0.166667h;

4-diethylaminoacetic acid [[11β,16α]-[[15,16-((R)-cyclohexylmethylene)bis(oxy)]-11-hydroxypregna-1,4-diene-3,20-dion-21-yl]] ester; With 1,2,2,6,6-pentamethylpiperidine; trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 20 ℃;

trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;