(R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate

Base Information

Chemical Name:(R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate
CAS No.:1313485-94-7
Molecular Formula:C₄₉H₇₄N₃O₁₀P
Molecular Weight:896.114
Hs Code.:

(R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate

Synonyms:(R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate

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Chemical Property of (R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate

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Technology Process of (R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate

There total 8 articles about (R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₉H₇₂N₃O₁₀P

: 1313485-94-7
(R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate

Guidance literature:: With sodium tetrahydroborate; water; In tetrahydrofuran; at 0 ℃; for 0.5h;

Reference yield:

: 1313485-91-4
(R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[3-[[(tert-butyldimethylsilyl)oxy]methyl]-4-hydroxyphenyl]-2-hydroxyethyl]carbamate

: 1313485-94-7
(R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C

2.1: manganese(IV) oxide / chloroform / 20 °C

3.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; Bromotrichloromethane / dichloromethane / 2 h / 0 - 20 °C

3.2: 3 h / 0 - 20 °C

4.1: water; sodium tetrahydroborate / tetrahydrofuran / 0.5 h / 0 °C

With manganese(IV) oxide; sodium tetrahydroborate; Bromotrichloromethane; tetrabutyl ammonium fluoride; N-benzyl-N,N,N-triethylammonium chloride; water; sodium hydroxide; In tetrahydrofuran; dichloromethane; chloroform;

Reference yield:

: 1313485-92-5
(R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-hydroxy-2-[4-hydroxy-3-(hydroxymethyl)phenyl]ethyl]carbamate

: 1313485-94-7
(R)-tert-butyl [9-[4-[[(1,1'-biphenyl)-2-ylcarbamoyl]oxy]piperidin-1-yl]nonyl][2-[4-[(di-tert-butoxyphosphoryl)oxy]-3-(hydroxymethyl)phenyl]-2-hydroxyethyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: manganese(IV) oxide / chloroform / 20 °C

2.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; Bromotrichloromethane / dichloromethane / 2 h / 0 - 20 °C

2.2: 3 h / 0 - 20 °C

3.1: water; sodium tetrahydroborate / tetrahydrofuran / 0.5 h / 0 °C

With manganese(IV) oxide; sodium tetrahydroborate; Bromotrichloromethane; N-benzyl-N,N,N-triethylammonium chloride; water; sodium hydroxide; In tetrahydrofuran; dichloromethane; chloroform;