2-iodo-4,6-dimethylphenyl methoxymethyl sulfide

Base Information

• Chemical Name: 2-iodo-4,6-dimethylphenyl methoxymethyl sulfide
• CAS No.: 1610038-83-9
• Molecular Formula: C₁₀H₁₃IOS
• Molecular Weight: 308.183
• Mol file: 1610038-83-9.mol

Synonyms:2-iodo-4,6-dimethylphenyl methoxymethyl sulfide

Chemical Property of 2-iodo-4,6-dimethylphenyl methoxymethyl sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-iodo-4,6-dimethylphenyl methoxymethyl sulfide

There total 1 articles about 2-iodo-4,6-dimethylphenyl methoxymethyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

2-iodo-4,6-dimethylaniline (4102-54-9) + potassium ethyl xanthogenate (140-89-6) → 2-iodo-4,6-dimethylphenyl methoxymethyl sulfide (1610038-83-9)

Guidance literature:

2-iodo-4,6-dimethylaniline; With isopentyl nitrite; In ethanol; water; at 0 ℃; for 0.333333h;

potassium ethyl xanthogenate; In acetone; at -40 - 0 ℃; for 1.33333h;

potassium ethyl xanthogenate; In acetone; at -40 - 0 ℃; for 1.33333h;

DOI:10.1039/c4ob00299g

Reference yield: 89.0%

2-iodo-4,6-dimethylphenyl methoxymethyl sulfide (1610038-83-9) + phenylacetylene (536-74-3) → 2,4-dimethyl-6-(phenylethynyl)phenyl methoxymethyl sulfide (1610038-76-0)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 20 ℃; for 2.5h; Inert atmosphere;

DOI:10.1039/c4ob00299g

upstream raw materials:

2-iodo-4,6-dimethylaniline

potassium ethyl xanthogenate

Downstream raw materials:

2,4-dimethyl-6-(phenylethynyl)phenyl methoxymethyl sulfide