N-(4-(2,7-dibromo-9H-carbazol-9-yl)phenyl)-N-phenylbenzenamine

Base Information

• Chemical Name: N-(4-(2,7-dibromo-9H-carbazol-9-yl)phenyl)-N-phenylbenzenamine
• CAS No.: 1303532-40-2
• Molecular Formula: C₃₀H₂₀Br₂N₂
• Molecular Weight: 568.31
• Mol file: 1303532-40-2.mol

Synonyms:N-(4-(2,7-dibromo-9H-carbazol-9-yl)phenyl)-N-phenylbenzenamine

Chemical Property of N-(4-(2,7-dibromo-9H-carbazol-9-yl)phenyl)-N-phenylbenzenamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(4-(2,7-dibromo-9H-carbazol-9-yl)phenyl)-N-phenylbenzenamine

There total 4 articles about N-(4-(2,7-dibromo-9H-carbazol-9-yl)phenyl)-N-phenylbenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

iodobenzene (591-50-4) + 2,7-dibromo-9-(4-aminophenyl)-9H-carbazole (568592-11-0) → N-(4-(2,7-dibromo-9H-carbazol-9-yl)phenyl)-N-phenylbenzenamine (1303532-40-2)

Guidance literature:

With 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide; In toluene; Reflux;

DOI:10.1016/j.polymer.2011.02.029

Reference yield:

4-Fluoronitrobenzene (350-46-9,178603-76-4) → N-(4-(2,7-dibromo-9H-carbazol-9-yl)phenyl)-N-phenylbenzenamine (1303532-40-2)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

2: hydrogenchloride; tin / ethanol; water / Reflux

3: 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide / toluene / Reflux

With hydrogenchloride; tin; 1,10-Phenanthroline; potassium carbonate; copper(l) chloride; potassium hydroxide; In ethanol; water; N,N-dimethyl-formamide; toluene;

DOI:10.1016/j.polymer.2011.02.029

Reference yield:

2,7-dibromo-9-(4-nitrophenyl)-9H-carbazole (568592-10-9) → N-(4-(2,7-dibromo-9H-carbazol-9-yl)phenyl)-N-phenylbenzenamine (1303532-40-2)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride; tin / ethanol; water / Reflux

2: 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide / toluene / Reflux

With hydrogenchloride; tin; 1,10-Phenanthroline; copper(l) chloride; potassium hydroxide; In ethanol; water; toluene;

DOI:10.1016/j.polymer.2011.02.029

upstream raw materials:

iodobenzene

2,7-dibromo-9-(4-aminophenyl)-9H-carbazole

2,7-dibromo-9H-carbazole

4-Fluoronitrobenzene

Downstream raw materials:

N-(4-(2,7-di(1,3,2-dioxaborinan-2-yl)-9H-carbazol-9-yl)phenyl)-N-phenylbenzenamine