Technology Process of 2-(2-oxopropyl)-3-<(benzyloxy)methyl>-4,4-dimethylcyclopentanone
There total 4 articles about 2-(2-oxopropyl)-3-<(benzyloxy)methyl>-4,4-dimethylcyclopentanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfuric acid; acetic acid;
at 70 - 80 ℃;
for 1h;
DOI:10.1021/jo00285a013
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / LiAlH4 / tetrahydrofuran / Ambient temperature
2: 1.) sodium hydride, tetra n-butylammonium iodide / 1.) THF, 30 min, 2.) room temp., 14 h
3: 82 percent / 80percent aq. acetic acid, conc. H2SO4 / 1 h / 70 - 80 °C
With
lithium aluminium tetrahydride; sulfuric acid; tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid;
In
tetrahydrofuran;
DOI:10.1021/jo00285a013
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) sodium hydride, tetra n-butylammonium iodide / 1.) THF, 30 min, 2.) room temp., 14 h
2: 82 percent / 80percent aq. acetic acid, conc. H2SO4 / 1 h / 70 - 80 °C
With
sulfuric acid; tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid;
DOI:10.1021/jo00285a013
