tert-butyl (1-(4-(4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutyl)carbamate

Base Information

• Chemical Name: tert-butyl (1-(4-(4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutyl)carbamate
• CAS No.: 1301610-60-5
• Molecular Formula: C₂₇H₂₇N₃O₄
• Molecular Weight: 457.529

Synonyms:tert-butyl (1-(4-(4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutyl)carbamate

Chemical Property of tert-butyl (1-(4-(4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutyl)carbamate

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Technology Process of tert-butyl (1-(4-(4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutyl)carbamate

There total 1 articles about tert-butyl (1-(4-(4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

tert-butyl 1-(4-(4-methoxy-5-phenylfuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutylcarbamate (1301611-89-1) → tert-butyl (1-(4-(4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutyl)carbamate (1301610-60-5)

Guidance literature:

With water; sodium hydroxide; In 1,4-dioxane; Reflux;

Reference yield: 80.0%

tert-butyl (1-(4-(4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutyl)carbamate (1301610-60-5) + cyclopropylcarbinyl bromide (7051-34-5) → tert-butyl 1-(4-(3-(cyclopropylmethyl)-4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutylcarbamate (1301612-24-7)

Guidance literature:

With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1h;

Reference yield: 80.0%

tert-butyl (1-(4-(4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutyl)carbamate (1301610-60-5) + methyl iodide (74-88-4) → tert-butyl 1-(4-(3-methyl-4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutylcarbamate (1301611-58-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

upstream raw materials:

tert-butyl 1-(4-(4-methoxy-5-phenylfuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutylcarbamate

Downstream raw materials:

tert-butyl 1-(4-(3-(cyclopropylmethyl)-4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutylcarbamate

tert-butyl 1-(4-(3-(2-methoxyethyl)-4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutylcarbamate

tert-butyl 1-(4-(3-(2-hydroxyethyl)-4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutylcarbamate

tert-butyl 1-(4-(3-methyl-4-oxo-5-phenyl-3,4-dihydrofuro[2,3-d]pyrimidin-6-yl)phenyl)cyclobutylcarbamate

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